Planilha de Destilação

Esta é uma pré-visualização de arquivo. Entre para ver o arquivo original

Dados e perfis
	Prática 5 - Destilação
	Calibração do picnômetro:	Massa de agua 
	Massa picnômetro vazio:	16.67	5.5
	Massa picnômetro + água:	22.17
	Temperatura ambiente:	25
	Temperatura em cada estágio
	Tempo	 Temperatura (°C)
	(min) 	9	8	7	6	5	4	3	2	1
	0	30	25	25	25	25	25	25	25	25
	15	88	76	66	69	65	58	60	59	60
	30	90	82	79	76	75	74	74	74	75
	45	95	90	86	85	82	76	75	73	72
	Massa em cada estágio
	Estágio 	Massa picnômetro + líquido	Massa da mistura 	Densidade 	Fração Molar x Etanol	Fração Molar x Água
	Balão (alimentação)	21.93	5.26	0.956	0.136491866	0.863508134
	Balão (final)	22.07	5.4	0.982	0.053824090	0.946175910
	Destilado (final)	21.12	4.45	0.809	0.838394618	0.161605382
	1	21.18	4.51	0.820	0.753649664	0.246350336
	2	21.23	4.56	0.829	0.690430935	0.309569065
	3	21.34	4.67	0.849	0.570552917	0.429447083
	4	21.44	4.77	0.867	0.478978121	0.521021879
	5	21.72	5.05	0.918	0.271288441	0.728711559
	6	21.93	5.26	0.956	0.136491866	0.863508134
	7	22.05	5.38	0.978	0.065127632	0.934872368
	8	22.05	5.38	0.978	0.065127632	0.934872368
	Estágio 	Massa picnômetro + líquido	Massa da mistura 	Densidade 	Fração Molar x Etanol	Fração Molar x Água
	Fundo - Balão	Início	21.93	5.26	0.956	0.1365	0.8635
	Final	22.07	5.4	0.982	0.0538	0.9462
	Topo - Destilado	Início	-	-	-	-	-
	Final	21.12	4.45	0.809	0.8384	0.1616
	A curva de calibração usada nos cálculos foi obtida na disciplina termodinâmica experimental: y = 426,582x4 - 1603,47x3 + 2263,83x2 - 1426,28x + 339,339
	Parâmetros 	Potência 
	a	426.58	4.00
	b	1,603.47	3.00
	c	2,263.83	2.00
	d	1,426.28	1.00
	e	339.34	-
TermoExp
	Massa das soluções (g)
	Identificação	Volume de água (mL)	Volume de etanol (mL)	1ª medida - M3 (g)	2ª medida - M3 (g)	Densidade - 1ª MEDIDA 	Densidade - 2ª MEDIDA	Diferença das densidades	Cálculo de Pureza do Etanol
	Solução 1	10.00	0.00	6.0536	6.0581	M2	1.0000	1.0000	0.0000	Substância	Fração Mássica	Volume	Fração Volumétrica
	Solução 2	9.00	1.00	5.9706	5.9795	M3	0.9863	0.9870	-0.0007	Etanol	0.928	118.217	0.942
	Solução 3	8.00	2.00	5.9023	5.9141	M3	0.9750	0.9762	-0.0012	Água	0.072	7.222	0.058
	Solução 4	7.00	3.00	5.8284	5.8388	M3	0.9628	0.9638	-0.0010
	Solução 5	6.00	4.00	5.7439	5.7872	M3	0.9488	0.9553	-0.0064	ρ água (25°C) g/cm³	0.997
	Solução 6	5.00	5.00	5.6514	5.6446	M3	0.9336	0.9317	0.0018	ρ etanol (25°C) g/cm³	0.785
	Solução 7	4.00	6.00	5.5140	5.5237	M3	0.9109	0.9118	-0.0009	MM Água (g/mol)	18.015
	Solução 8	3.00	7.00	5.4002	5.4003	M3	0.8921	0.8914	0.0006	MM Etanol (g/mol)	46.068
	Solução 9	2.00	8.00	5.2349	5.2443	M3	0.8648	0.8657	-0.0009	Grau de Pureza Álcool (I.N.P.M)	92.8º
	Solução 10	1.00	9.00	5.0814	5.0670	M3	0.8394	0.8364	0.0030
	Solução 11	0.00	10.00	4.8951	4.9061	M3	0.8086	0.8098	-0.0012	92.8º = 92.8 g em 100 g de mistura
	Incerteza das densidades	0.0017
	0.0023
	Identificação	Volume de etanol 
corrigido (mL)	Volume de água
corrigido (mL)	Volume total 
de água (mL)	Massa total de água (g)	Massa total de etanol (g)	Número de mols de água	Número de mols de etanol	Fração molar de água	Fração molar de etanol
	Solução 1	0.00	0.00	10.00	9.9700	0.0000	0.5534	0.0000	1.0000	0.0000	1	1.0023	0.9977	0
	Solução 2	0.94	0.06	9.06	9.0304	0.7398	0.5013	0.0161	0.9690	0.0310	0.9900285473	0.9923	0.9877	-0.0003216598
	Solução 3	1.88	0.12	8.12	8.0908	1.4796	0.4491	0.0321	0.9333	0.0667	0.9788810261	0.9812	0.9766	-0.0010252905
	Solução 4	2.83	0.17	7.17	7.1512	2.2194	0.3970	0.0482	0.8918	0.1082	0.9694523743	0.9718	0.9671	-0.0006634233
	Solução 5	3.77	0.23	6.23	6.2116	2.9592	0.3448	0.0642	0.8430	0.1570	0.954666077	0.9570	0.9523	-0.0012464316
	Solução 6	4.71	0.29	5.29	5.2720	3.6990	0.2926	0.0803	0.7847	0.2153	0.9382212215	0.9405	0.9359	-0.0016082988
	Solução 7	5.65	0.35	4.35	4.3324	4.4388	0.2405	0.0964	0.7139	0.2861	0.9200977042	0.9224	0.9178	-0.0012263279
	Solução 8	6.60	0.40	3.40	3.3928	5.1786	0.1883	0.1124	0.6262	0.3738	0.8997929315	0.9021	0.8975	-0.0017088175
	Solução 9	7.54	0.46	2.46	2.4532	5.9185	0.1362	0.1285	0.5146	0.4854	0.8767942584	0.8791	0.8745	-0.0003417635
	Solução 10	8.48	0.52	1.52	1.5136	6.6583	0.0840	0.1445	0.3676	0.6324	0.8465180331	0.8488	0.8442	-0.0019902698
	Solução 11	9.42	0.58	0.58	0.5740	7.3981	0.0319	0.1606	0.1656	0.8344	0.8285855012	0.8309	0.8263	-0.0019902698
	Ajustes Polinomiais
	Incerteza expandida da fração molar associada a massa
	Identificação	Fração molar de Etanol	Média das densidades	Ajuste de 1ª ordem	Ajuste de 2ª ordem	Ajuste de 3ª ordem	Ajuste de 4ª ordem	Resíduo 1ª ordem	Resíduo 2ª ordem	Resíduo 3ª ordem	Residuo 4	INCERTEZA ÁGUA	INCERTEZA ETANOL
	Solução 1	0.0000	1.0000	-0.0436	0.0070	-0.0130	0.0010	0.0436	-0.0070	0.0130	-0.0010	0.0000288863	0
	Solução 2	0.0310	0.9867	0.0124	0.0388	0.0316	0.0391	0.0186	-0.0078	-0.0006	-0.0081	0.0000308718	0.0000042122
	Solução 3	0.0667	0.9756	0.0587	0.0680	0.0676	0.0732	0.0080	-0.0012	-0.0009	-0.0065	0.0000331467	0.0000045965
	Solução 4	0.1082	0.9633	0.1105	0.1035	0.1073	0.1132	-0.0022	0.0047	0.0009	-0.0050	0.0000357762	0.0000051376
	Solução 5	0.1570	0.9521	0.1576	0.1387	0.1437	0.1511	-0.0006	0.0183	0.0134	0.0059	0.000038845	0.0000059496
	Solução 6	0.2153	0.9327	0.2391	0.2058	0.2082	0.2189	-0.0238	0.0095	0.0071	-0.0036	0.0000424632	0.0000072474
	Solução 7	0.2861	0.9113	0.3286	0.2887	0.2844	0.2968	-0.0426	-0.0027	0.0017	-0.0107	0.0000467701	0.000009451
	Solução 8	0.3738	0.8917	0.4108	0.3732	0.3618	0.3729	-0.0371	0.0006	0.0120	0.0009	0.000051927	0.0000134447
	Solução 9	0.4854	0.8652	0.5222	0.5006	0.4830	0.4887	-0.0368	-0.0151	0.0024	-0.0033	0.0000580463	0.0000213612
	Solução 10	0.6324	0.8379	0.6369	0.6472	0.6335	0.6347	-0.0045	-0.0148	-0.0011	-0.0023	0.0000647826	0.0000397156
	Solução 11	0.8344	0.8092	0.7572	0.8179	0.8272	0.8372	0.0772	0.0165	0.0072	-0.0028	0.0000685107	0.0001001593
	fração molar calculada - incerteza da fraçao molar - eixo y
	Incerteza expandida da fração molar associada ao volume
	δx etanol	δx água
	0.0018746749	0.0086361933
	0.0020208841	0.0073539171
	0.0021951135	0.0075054509
	0.0024053045	0.0079762735
	0.0026631385	0.0086338247
	0.0029872017	0.0094774279
	0.0034113492	0.0105518236
	0.0040149783	0.0119415208
	0.0051011268	0.0137908092
	0.0098459125	0.0163553442
Equilibrio
	Dados:
	Reta 45 °C
	X Etanol	Y Etanol	T (K)	X Água	Y Água	0	0
	1	1
	0.00006350	0.00067790	372.85	0.99993650	0.99932210
	0.00024620	0.00262190	372.80	0.99975380	0.99737810
	0.00042960	0.00456330	372.75	0.99957040	0.99543670
	0.00061370	0.00650200	372.70	0.99938630	0.99349800
	0.00079850	0.00843810	372.65	0.99920150	0.99156190
	0.00098400	0.01037150	372.60	0.99901600	0.98962850
	0.00117010	0.01230240	372.55	0.99882990	0.98769760
	0.00135700	0.01423060	372.50	0.99864300	0.98576940
	0.00154450	0.01615610	372.45	0.99845550	0.98384390
	0.00173280	0.01807910	372.40	0.99826720	0.98192090
	0.00192180	0.01999940	372.35	0.99807820	0.98000060
	0.00211150	0.02191710	372.30	0.99788850	0.97808290
	0.00230190	0.02383230	372.25	0.99769810	0.97616770
	0.00249300	0.02574480	372.20	0.99750700	0.97425520
	0.00268490	0.02765470	372.15	0.99731510	0.97234530
	0.00287750	0.02956200	372.10	0.99712250	0.97043800
	0.00307080	0.03146670	372.05	0.99692920	0.96853330
	0.00326480	0.03336890	372.00	0.99673520	0.96663110
	0.00345970	0.03526840	371.95	0.99654030	0.96473160
	0.00365520	0.03716540	371.90	0.99634480	0.96283460
	0.00385150	0.03905980	371.85	0.99614850	0.96094020
	0.00404860	0.04095160	371.80	0.99595140	0.95904840
	0.00424640	0.04284080	371.75	0.99575360	0.95715920
	0.00444500	0.04472750	371.70	0.99555500	0.95527250
	0.00464440	0.04661150	371.65	0.99535560	0.95338850
	0.00484450	0.04849310	371.60	0.99515550	0.95150690
	0.00504550	0.05037210	371.55	0.99495450	0.94962790
	0.00524720	0.05224850	371.50	0.99475280	0.94775150
	0.00544970	0.05412230	371.45	0.99455030	0.94587770
	0.00565300	0.05599360	371.40	0.99434700	0.94400640
	0.00585710	0.05786240	371.35	0.99414290	0.94213760
	0.00606200	0.05972860
371.30	0.99393800	0.94027140
	0.00626770	0.06159230	371.25	0.99373230	0.93840770
	0.00647430	0.06345350	371.20	0.99352570	0.93654650
	0.00668160	0.06531210	371.15	0.99331840	0.93468790
	0.00688980	0.06716820	371.10	0.99311020	0.93283180
	0.00709880	0.06902180	371.05	0.99290120	0.93097820
	0.00730870	0.07087290	371.00	0.99269130	0.92912710
	0.00751940	0.07272140	370.95	0.99248060	0.92727860
	0.00773090	0.07456740	370.90	0.99226910	0.92543260
	0.00794330	0.07641090	370.85	0.99205670	0.92358910
	0.00815650	0.07825190	370.80	0.99184350	0.92174810
	0.00837070	0.08009040	370.75	0.99162930	0.91990960
	0.00858560	0.08192640	370.70	0.99141440	0.91807360
	0.00880150	0.08376000	370.65	0.99119850	0.91624000
	0.00901820	0.08559100	370.60	0.99098180	0.91440900
	0.00923590	0.08741950	370.55	0.99076410	0.91258050
	0.00945440	0.08924560	370.50	0.99054560	0.91075440
	0.00967380	0.09106910	370.45	0.99032620	0.90893090
	0.00989410	0.09289020	370.40	0.99010590	0.90710980
	0.01011530	0.09470880	370.35	0.98988470	0.90529120
	0.01033740	0.09652500	370.30	0.98966260	0.90347500
	0.01056050	0.09833870	370.25	0.98943950	0.90166130
	0.01078450	0.10014990	370.20	0.98921550	0.89985010
	0.01100940	0.10195870	370.15	0.98899060	0.89804130
	0.01123530	0.10376500	370.10	0.98876470	0.89623500
	0.01146210	0.10556880	370.05	0.98853790	0.89443120
	0.01168980	0.10737020	370.00	0.98831020	0.89262980
	0.01191850	0.10916920	369.95	0.98808150	0.89083080
	0.01214820	0.11096570	369.90	0.98785180	0.88903430
	0.01237880	0.11275980	369.85	0.98762120	0.88724020
	0.01261050	0.11455150	369.80	0.98738950	0.88544850
	0.01284310	0.11634070	369.75	0.98715690	0.88365930
	0.01307670	0.11812750	369.70	0.98692330	0.88187250
	0.01331130	0.11991190	369.65	0.98668870	0.88008810
	0.01354690	0.12169380	369.60	0.98645310	0.87830620
	0.01378350	0.12347340	369.55	0.98621650	0.87652660
	0.01402110	0.12525050	369.50	0.98597890	0.87474950
	0.01425980	0.12702520	369.45	0.98574020	0.87297480
	0.01449940	0.12879760	369.40	0.98550060	0.87120240
	0.01474020	0.13056750	369.35	0.98525980	0.86943250
	0.01498190	0.13233500	369.30	0.98501810	0.86766500
	0.01522470	0.13410020	369.25	0.98477530	0.86589980
	0.01546860	0.13586290	369.20	0.98453140	0.86413710
	0.01571360	0.13762330	369.15	0.98428640	0.86237670
	0.01595960	0.13938130	369.10	0.98404040	0.86061870
	0.01620670	0.14113690	369.05	0.98379330	0.85886310
	0.01645490	0.14289010	369.00	0.98354510	0.85710990
	0.01670420	0.14464100	368.95	0.98329580	0.85535900
	0.01695460	0.14638950	368.90	0.98304540	0.85361050
	0.01720610	0.14813570	368.85	0.98279390	0.85186430
	0.01745880	0.14987950	368.80	0.98254120	0.85012050
	0.01771250	0.15162090	368.75	0.98228750	0.84837910
	0.01796740	0.15336000	368.70	0.98203260	0.84664000
	0.01822350	0.15509680	368.65	0.98177650	0.84490320
	0.01848070	0.15683120	368.60	0.98151930	0.84316880
	0.01873910	0.15856330	368.55	0.98126090	0.84143670
	0.01899860	0.16029300	368.50	0.98100140	0.83970700
	0.01925930	0.16202040	368.45	0.98074070	0.83797960
	0.01952130	0.16374550	368.40	0.98047870	0.83625450
	0.01978440	0.16546830	368.35	0.98021560	0.83453170
	0.02004870	0.16718870	368.30	0.97995130	0.83281130
	0.02031420	0.16890690	368.25	0.97968580	0.83109310
	0.02058100	0.17062270	368.20	0.97941900	0.82937730
	0.02084900	0.17233620	368.15	0.97915100	0.82766380
	0.02111820	0.17404740	368.10	0.97888180	0.82595260
	0.02138870	0.17575640	368.05	0.97861130	0.82424360
	0.02166040	0.17746300	368.00	0.97833960	0.82253700
	0.02193340	0.17916730	367.95	0.97806660	0.82083270
	0.02220770	0.18086940	367.90	0.97779230	0.81913060
	0.02248330	0.18256920	367.85	0.97751670	0.81743080
	0.02276020	0.18426670	367.80	0.97723980	0.81573330
	0.02303840	0.18596190	367.75	0.97696160	0.81403810
	0.02331790	0.18765490	367.70	0.97668210	0.81234510
	0.02359870	0.18934560	367.65	0.97640130	0.81065440
	0.02388090	0.19103410	367.60	0.97611910	0.80896590
	0.02416440	0.19272020	367.55	0.97583560	0.80727980
	0.02444930	0.19440420	367.50	0.97555070	0.80559580
	0.02473560	0.19608590	367.45	0.97526440	0.80391410
	0.02502320	0.19776530	367.40	0.97497680	0.80223470
	0.02531220	0.19944250	367.35	0.97468780	0.80055750
	0.02560270	0.20111750	367.30	0.97439730	0.79888250
	0.02589450	0.20279030	367.25	0.97410550	0.79720970
	0.02618780	0.20446080	367.20	0.97381220	0.79553920
	0.02648250	0.20612910	367.15	0.97351750	0.79387090
	0.02677870	0.20779520	367.10	0.97322130	0.79220480
	0.02707630	0.20945910	367.05	0.97292370	0.79054090
	0.02737540	0.21112070	367.00	0.97262460	0.78887930
	0.02767600	0.21278020	366.95	0.97232400	0.78721980
	0.02797810	0.21443750	366.90	0.97202190	0.78556250
	0.02828160	0.21609250	366.85	0.97171840	0.78390750
	0.02858670	0.21774540	366.80	0.97141330	0.78225460
	0.02889340	0.21939610	366.75	0.97110660	0.78060390
	0.02920160	0.22104460	366.70	0.97079840	0.77895540
	0.02951130	0.22269100	366.65	0.97048870	0.77730900
	0.02982260	0.22433510	366.60	0.97017740	0.77566490
	0.03013550	0.22597710	366.55	0.96986450	0.77402290
	0.03045000	0.22761700	366.50	0.96955000	0.77238300
	0.03076610	0.22925460	366.45	0.96923390	0.77074540
	0.03108380	0.23089020	366.40	0.96891620	0.76910980
	0.03140320	0.23252350	366.35	0.96859680	0.76747650
	0.03172420	0.23415480	366.30	0.96827580	0.76584520
	0.03204690	0.23578380	366.25	0.96795310	0.76421620
	0.03237120	0.23741080	366.20	0.96762880	0.76258920
	0.03269730	0.23903560	366.15	0.96730270	0.76096440
	0.03302510	0.24065830	366.10	0.96697490	0.75934170
	0.03335460	0.24227890	366.05	0.96664540	0.75772110
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363.70	0.94889490	0.68385310
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356.10	0.80845470	0.46677830
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	0.48557510	0.64295490	353.05	0.51442490	0.35704510
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	0.52681440	0.65845490	352.80	0.47318560	0.34154510
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	0.61766900	0.69939020	352.30	0.38233100	0.30060980
	0.62768310	0.70456920	352.25	0.37231690	0.29543080
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	0.64847740	0.71578830	352.15	0.35152260	0.28421170
	0.65932330	0.72189510	352.10	0.34067670	0.27810490
	0.67052250	0.72838840	352.05	0.32947750	0.27161160
	0.68212640	0.73532030	352.00	0.31787360	0.26467970
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	0.73410490	0.76897810	351.80	0.26589510	0.23102190
	0.74907620	0.77947410	351.75	0.25092380	0.22052590
	0.76521950	0.79119400	351.70	0.23478050	0.20880600
	0.78286530	0.80447840	351.65	0.21713470	0.19552160
	0.80250960	0.81983960	351.60	0.19749040	0.18016040
	0.82494690	0.83810120	351.55	0.17505310	0.16189880
	0.85156870	0.86070920	351.50	0.14843130	0.13929080
	0.88511230	0.89051920	351.45	0.11488770	0.10948080
	0.93156730	0.93380720	351.40	0.06843270	0.06619280
	0.99813010	0.99818030	351.35	0.00186990	0.00181970