AMOSTA DE AGUA Pb 25 09 2017

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Method: Cleide 26-01-17 Page 1 Date: 25/9/2017 16:13:25 
 
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Analysis Begun
 
Logged In Analyst: Lab. Instrumental Technique: AA Flame
Spectrometer Model: AAnalyst 400, S/N 201S9070605 Autosampler Model: S10
 
Sample Information File: C:\data-AA\Lab. Instrumental\Sample Information\ANALISE DE AGUA TULIO 25 09 2017
Batch ID: 
Results Data Set: 
Results Library: 
 
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Method Loaded
Method Name: Cleide 26-01-17 Method Last Saved: 24/8/2017 17:25:49
Method Description: 
 
====================================================================================================
Sequence No.: 1 Autosampler Location: 
Sample ID: Branco Date Collected: 25/9/2017 15:35:58
Analyst: Data Type: Original
 
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Replicate Data: Branco
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.00] 0.296 15:36:01 No
 2 [0.00] 0.296 15:36:06 No
 3 [0.00] 0.296 15:36:10 No
 4 [0.00] 0.296 15:36:14 No
 5 [0.00] 0.296 15:36:19 No
Mean: [0.00] 0.296
SD: 0.00 0.0002
%RSD: 0.00 0.07
Auto-zero performed.
 
====================================================================================================
Sequence No.: 2 Autosampler Location: 
Sample ID: Branco Date Collected: 25/9/2017 15:36:34
Analyst: Data Type: Original
 
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Replicate Data: Branco
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.00] -0.000 15:36:35 No
 2 [0.00] 0.000 15:36:40 No
 3 [0.00] 0.000 15:36:44 No
 4 [0.00] 0.001 15:36:48 No
 5 [0.00] 0.000 15:36:53 No
Mean: [0.00] 0.000
SD: 0.00 0.0003
%RSD: 0.00 103.96
Auto-zero performed.
 
====================================================================================================
Sequence No.: 3 Autosampler Location: 
Sample ID: Branco Date Collected: 25/9/2017 15:36:59
Analyst: Data Type: Original
 
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Replicate Data: Branco
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.00] -0.000 15:36:59 No
 2 [0.00] -0.001 15:37:03 No
 3 [0.00] 0.000 15:37:07 No
 4 [0.00] -0.000 15:37:12 No
 5 [0.00] -0.001 15:37:16 No
Mean: [0.00] -0.000
SD: 0.00 0.0003
%RSD: 0.00 112.29
Method: Cleide 26-01-17 Page 2 Date: 25/9/2017 16:13:25 
Auto-zero performed.
 
====================================================================================================
Sequence No.: 4 Autosampler Location: 
Sample ID: Branco Date Collected: 25/9/2017 15:37:23
Analyst: Data Type: Original
 
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Replicate Data: Branco
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.00] -0.000 15:37:27 No
 2 [0.00] -0.001 15:37:31 No
 3 [0.00] -0.000 15:37:35 No
 4 [0.00] -0.001 15:37:40 No
 5 [0.00] -0.001 15:37:44 No
Mean: [0.00] -0.001
SD: 0.00 0.0005
%RSD: 0.00 66.72
Auto-zero performed.
 
====================================================================================================
Sequence No.: 5 Autosampler Location: 
Sample ID: Branco Date Collected: 25/9/2017 15:37:52
Analyst: Data Type: Original
 
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Replicate Data: Branco
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.00] -0.000 15:37:52 No
 2 [0.00] -0.000 15:37:57 No
 3 [0.00] -0.000 15:38:01 No
 4 [0.00] -0.001 15:38:05 No
 5 [0.00] -0.000 15:38:10 No
Mean: [0.00] -0.000
SD: 0.00 0.0001
%RSD: 0.00 37.14
Auto-zero performed.
 
====================================================================================================
Sequence No.: 6 Autosampler Location: 
Sample ID: 0.2 Date Collected: 25/9/2017 15:38:29
Analyst: Data Type: Original
 
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Replicate Data: 0.2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.2] 0.002 15:38:31 No
 2 [0.2] 0.002 15:38:35 No
 3 [0.2] 0.002 15:38:40 No
 4 [0.2] 0.001 15:38:44 No
 5 [0.2] 0.001 15:38:48 No
Mean: [0.2] 0.002
SD: 0.0 0.0002
%RSD: 0.0 15.27
Standard number 1 applied. [0.2]
Correlation Coef.: 1.000000 Slope: 0.00790 Intercept: 0.00000
 
====================================================================================================
Sequence No.: 7 Autosampler Location: 
Sample ID: 0.4 Date Collected: 25/9/2017 15:39:57
Analyst: Data Type: Original
 
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Replicate Data: 0.4
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.4] 0.003 15:39:58 No
 2 [0.4] 0.004 15:40:02 No
 3 [0.4] 0.004 15:40:07 No
Method: Cleide 26-01-17 Page 3 Date: 25/9/2017 16:13:25 
 4 [0.4] 0.004 15:40:11 No
 5 [0.4] 0.00415:40:15 No
Mean: [0.4] 0.004
SD: 0.0 0.0002
%RSD: 0.0 4.33
Standard number 2 applied. [0.4]
Correlation Coef.: 1.000000 Slope: 0.00696 Intercept: 0.00000
 
====================================================================================================
Sequence No.: 8 Autosampler Location: 
Sample ID: 0.6 Date Collected: 25/9/2017 15:41:23
Analyst: Data Type: Original
 
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Replicate Data: 0.6
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.6] 0.006 15:41:24 No
 2 [0.6] 0.006 15:41:28 No
 3 [0.6] 0.006 15:41:33 No
 4 [0.6] 0.006 15:41:37 No
 5 [0.6] 0.006 15:41:41 No
Mean: [0.6] 0.006
SD: 0.0 0.0001
%RSD: 0.0 2.18
Standard number 3 applied. [0.6]
Correlation Coef.: 0.998565 Slope: 0.00744 Intercept: 0.00000
 S-shaped calibration curve detected. Two-coefficient equation used.
 
====================================================================================================
Sequence No.: 9 Autosampler Location: 
Sample ID: 0.8 Date Collected: 25/9/2017 15:42:44
Analyst: Data Type: Original
 
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Replicate Data: 0.8
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [0.8] 0.008 15:42:45 No
 2 [0.8] 0.008 15:42:49 No
 3 [0.8] 0.008 15:42:54 No
 4 [0.8] 0.008 15:42:58 No
 5 [0.8] 0.008 15:43:02 No
Mean: [0.8] 0.008
SD: 0.0 0.0002
%RSD: 0.0 2.29
Standard number 4 applied. [0.8]
Correlation Coef.: 0.999984 Slope: 0.00455 Intercept: 0.00000
 
====================================================================================================
Sequence No.: 10 Autosampler Location: 
Sample ID: 1.0 Date Collected: 25/9/2017 15:43:53
Analyst: Data Type: Original
 
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Replicate Data: 1.0
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 [1.0] 0.010 15:43:55 No
 2 [1.0] 0.010 15:43:59 No
 3 [1.0] 0.010 15:44:03 No
 4 [1.0] 0.010 15:44:08 No
 5 [1.0] 0.010 15:44:12 No
Mean: [1.0] 0.010
SD: 0.0 0.0001
%RSD: 0.0 1.15
Standard number 5 applied. [1.0]
Correlation Coef.: 0.997730 Slope: 0.00807 Intercept: 0.00000
 S-shaped calibration curve detected. Two-coefficient equation used.
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Calibration data for Pb 283.31 Equation: Nonlinear Through Zero
Method: Cleide 26-01-17 Page 4 Date: 25/9/2017 16:13:25 
 Entered Calculated
 Mean Signal Conc. Conc. Standard
 ID (Abs) mg/L mg/L Deviation %RSD
 Branco 0.0000 0 0.000 0.00 37.1 
 0.2 0.0016 0.2 0.188 0.00 15.3 
 0.4 0.0036 0.4 0.414 0.00 4.3 
 0.6 0.0057 0.6 0.619 0.00 2.2 
 0.8 0.0078 0.8 0.811 0.00 2.3 
 1.0 0.0097 1.0 0.969 0.00 1.2 
Correlation Coef.: 0.997730 Slope: 0.00807 Intercept: 0.00000
 
====================================================================================================
Sequence No.: 11 Autosampler Location: 
Sample ID: A1 Date Collected: 25/9/2017 15:45:07
Analyst: Data Type: Original
 
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Replicate Data: A1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -0.591 -0.591 -0.004 15:45:09 No
 2 -0.582 -0.582 -0.004 15:45:13 No
 3 -0.590 -0.590 -0.004 15:45:17 No
 4 -0.596 -0.596 -0.004 15:45:22 No
 5 -0.576 -0.576 -0.004 15:45:26 No
Mean: -0.587 -0.587 -0.004
SD: 0.008 0.008 0.0001
%RSD: 1.340 1.340 1.20
 
====================================================================================================
Sequence No.: 12 Autosampler Location: 
Sample ID: A2 Date Collected: 25/9/2017 15:46:23
Analyst: Data Type: Original
 
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Replicate Data: A2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -0.747 -0.747 -0.005 15:46:25 No
 2 -0.706 -0.706 -0.005 15:46:29 No
 3 -0.755 -0.755 -0.005 15:46:33 No
 4 -0.754 -0.754 -0.005 15:46:38 No
 5 -0.801 -0.801 -0.006 15:46:42 No
Mean: -0.753 -0.753 -0.005
SD: 0.034 0.034 0.0002
%RSD: 4.481 4.481 3.89
 
====================================================================================================
Sequence No.: 13 Autosampler Location: 
Sample ID: A3 Date Collected: 25/9/2017 15:47:17
Analyst: Data Type: Original
 
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Replicate Data: A3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -0.830 -0.830 -0.006 15:47:18 No
 2 -0.831 -0.831 -0.006 15:47:23 No
 3 -0.844 -0.844 -0.006 15:47:27 No
 4 -0.865 -0.865 -0.006 15:47:31 No
 5 -0.858 -0.858 -0.006 15:47:35 No
Mean: -0.846 -0.846 -0.006
SD: 0.016 0.016 0.0001
%RSD: 1.870 1.870 1.59
 
====================================================================================================
Sequence No.: 14 Autosampler Location: 
Sample ID: B1 Date Collected: 25/9/2017 15:48:28
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------Replicate Data: B1
Method: Cleide 26-01-17 Page 5 Date: 25/9/2017 16:13:25 
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -0.899 -0.899 -0.006 15:48:30 No
 2 -0.889 -0.889 -0.006 15:48:34 No
 3 -0.925 -0.925 -0.006 15:48:38 No
 4 -0.948 -0.948 -0.006 15:48:43 No
 5 -0.933 -0.933 -0.006 15:48:47 No
Mean: -0.919 -0.919 -0.006
SD: 0.025 0.025 0.0001
%RSD: 2.674 2.674 2.25
 
====================================================================================================
Sequence No.: 15 Autosampler Location: 
Sample ID: B2 Date Collected: 25/9/2017 15:49:33
Analyst: Data Type: Original
 
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Replicate Data: B2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.021 -1.021 -0.007 15:49:34 No
 2 -1.017 -1.017 -0.007 15:49:39 No
 3 -1.030 -1.030 -0.007 15:49:43 No
 4 -1.039 -1.039 -0.007 15:49:47 No
 5 -1.020 -1.020 -0.007 15:49:52 No
Mean: -1.026 -1.026 -0.007
SD: 0.009 0.009 0.0000
%RSD: 0.882 0.882 0.73
 
====================================================================================================
Sequence No.: 16 Autosampler Location: 
Sample ID: B3 Date Collected: 25/9/2017 15:50:28
Analyst: Data Type: Original
 
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Replicate Data: B3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.100 -1.100 -0.007 15:50:29 No
 2 -1.069 -1.069 -0.007 15:50:33 No
 3 -1.071 -1.071 -0.007 15:50:38 No
 4 -1.134 -1.134 -0.007 15:50:42 No
 5 -1.148 -1.148 -0.008 15:50:46 No
Mean: -1.104 -1.104 -0.007
SD: 0.036 0.036 0.0002
%RSD: 3.256 3.256 2.66
 
====================================================================================================
Sequence No.: 17 Autosampler Location: 
Sample ID: C1 Date Collected: 25/9/2017 15:51:31
Analyst: Data Type: Original
 
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Replicate Data: C1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.091 -1.091 -0.007 15:51:33 No
 2 -1.264 -1.264 -0.008 15:51:37 No
 3 -1.220 -1.220 -0.008 15:51:41 No
 4 -1.201 -1.201 -0.008 15:51:45 No
 5 -1.283 -1.283 -0.008 15:51:50 No
Mean: -1.212 -1.212 -0.008
SD: 0.075 0.075 0.0004
%RSD: 6.199 6.199 5.02
 
====================================================================================================
Sequence No.: 18 Autosampler Location: 
Sample ID: C2 Date Collected: 25/9/2017 15:52:26
Analyst: Data Type: Original
 
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Replicate Data: C2
Method: Cleide 26-01-17 Page 6 Date: 25/9/2017 16:13:25 
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.294 -1.294 -0.008 15:52:27 No
 2 -1.302 -1.302 -0.008 15:52:32 No
 3 -1.264 -1.264 -0.008 15:52:36 No
 4 -1.298 -1.298 -0.008 15:52:41 No
 5 -1.290 -1.290 -0.008 15:52:45 No
Mean: -1.290 -1.290 -0.008
SD: 0.015 0.015 0.0001
%RSD: 1.164 1.164 0.92
 
====================================================================================================
Sequence No.: 19 Autosampler Location: 
Sample ID: C3 Date Collected: 25/9/2017 15:53:27
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: C3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.471 -1.471 -0.009 15:53:29 No
 2 -1.420 -1.420 -0.009 15:53:33 No
 3 -1.424 -1.424 -0.009 15:53:38 No
 4 -1.435 -1.435 -0.009 15:53:42 No
 5 -1.400 -1.400 -0.009 15:53:46 No
Mean: -1.430 -1.430 -0.009
SD: 0.026 0.026 0.0001
%RSD: 1.828 1.828 1.41
 
====================================================================================================
Sequence No.: 20 Autosampler Location: 
Sample ID: D1 Date Collected: 25/9/2017 15:54:35
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: D1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.667 -1.667 -0.010 15:54:36 No
 2 -1.643 -1.643 -0.010 15:54:40 No
 3 -1.548 -1.548 -0.009 15:54:45 No
 4 -1.610 -1.610 -0.010 15:54:49 No
 5 -1.644 -1.644 -0.010 15:54:53 No
Mean: -1.622 -1.622 -0.010
SD: 0.046 0.046 0.0002
%RSD: 2.839 2.839 2.15
 
====================================================================================================
Sequence No.: 21 Autosampler Location: 
Sample ID: D2 Date Collected: 25/9/2017 15:55:30
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: D2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.609 -1.609 -0.010 15:55:32 No
 2 -1.698 -1.698 -0.010 15:55:36 No
 3 -1.657 -1.657 -0.010 15:55:41 No
 4 -1.682 -1.682 -0.010 15:55:45 No
 5 -1.639 -1.639 -0.010 15:55:49 No
Mean: -1.657 -1.657 -0.010
SD: 0.035 0.035 0.0002
%RSD: 2.102 2.102 1.57
 
====================================================================================================
Sequence No.: 22 Autosampler Location: 
Sample ID: D3 Date Collected: 25/9/2017 15:56:34
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------Replicate Data: D3
Method: Cleide 26-01-17 Page 7 Date: 25/9/2017 16:13:25 
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.850 -1.850 -0.011 15:56:36 No
 2 -1.886 -1.886 -0.011 15:56:40 No
 3 -1.873 -1.873 -0.011 15:56:44 No
 4 -1.897 -1.897 -0.011 15:56:49 No
 5 -1.904 -1.904 -0.011 15:56:53 No
Mean: -1.882 -1.882 -0.011
SD: 0.021 0.021 0.0001
%RSD: 1.127 1.127 0.82
 
====================================================================================================
Sequence No.: 23 Autosampler Location: 
Sample ID: E1 Date Collected: 25/9/2017 15:57:30
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: E1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -1.964 -1.964 -0.011 15:57:31 No
 2 -1.962 -1.962 -0.011 15:57:36 No
 3 -1.929 -1.929 -0.011 15:57:40 No
 4 -1.923 -1.923 -0.011 15:57:44 No
 5 -1.919 -1.919 -0.011 15:57:49 No
Mean: -1.939 -1.939 -0.011
SD: 0.022 0.022 0.0001
%RSD: 1.131 1.131 0.81
 
====================================================================================================
Sequence No.: 24 Autosampler Location: 
Sample ID: E2 Date Collected: 25/9/2017 15:58:18
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: E2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.086 -2.086 -0.012 15:58:20 No
 2 -2.001 -2.001 -0.011 15:58:24 No
 3 -2.081 -2.081 -0.012 15:58:28 No
 4 -2.035 -2.035 -0.012 15:58:32 No
 5 -2.083 -2.083 -0.012 15:58:37 No
Mean: -2.057 -2.057 -0.012
SD: 0.038 0.038 0.0002
%RSD: 1.833 1.833 1.30
 
====================================================================================================
Sequence No.: 25 Autosampler Location: 
Sample ID: E3 Date Collected: 25/9/2017 15:59:22
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: E3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.146 -2.146 -0.012 15:59:24 No
 2 -2.167 -2.167 -0.012 15:59:28 No
 3 -2.189 -2.189 -0.012 15:59:33 No
 4 -2.095 -2.095 -0.012 15:59:37 No
 5 -2.211 -2.211 -0.012 15:59:41 No
Mean: -2.162 -2.162 -0.012
SD: 0.044 0.044 0.0002
%RSD: 2.047 2.047 1.43
 
====================================================================================================
Sequence No.: 26 Autosampler Location: 
Sample ID: F1 Date Collected: 25/9/2017 16:00:23
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: F1
Method: Cleide 26-01-17 Page 8 Date: 25/9/2017 16:13:25 
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.291 -2.291 -0.013 16:00:24 No
 2 -2.355 -2.355 -0.013 16:00:28 No
 3 -2.247 -2.247 -0.012 16:00:33 No
 4 -2.333 -2.333 -0.013 16:00:37 No
 5 -2.328 -2.328 -0.013 16:00:41 No
Mean: -2.311 -2.311 -0.013
SD: 0.042 0.042 0.0002
%RSD: 1.828 1.828 1.25
 
====================================================================================================
Sequence No.: 27 Autosampler Location: 
Sample ID: F2 Date Collected: 25/9/2017 16:01:16
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: F2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.325 -2.325 -0.013 16:01:18 No
 2 -2.328 -2.328 -0.013 16:01:22 No
 3 -2.371 -2.371 -0.013 16:01:26 No
 4 -2.343 -2.343 -0.013 16:01:31 No
 5 -2.404 -2.404 -0.013 16:01:35 No
Mean: -2.354 -2.354 -0.013
SD: 0.033 0.033 0.0001
%RSD: 1.411 1.411 0.95
 
====================================================================================================
Sequence No.: 28 Autosampler Location: 
Sample ID: F3 Date Collected: 25/9/2017 16:02:14
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: F3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.416 -2.416 -0.013 16:02:16 No
 2 -2.587 -2.587 -0.014 16:02:20 No
 3 -2.523 -2.523 -0.013 16:02:25 No
 4 -2.624 -2.624 -0.014 16:02:29 No
 5 -2.511 -2.511 -0.013 16:02:33 No
Mean: -2.532 -2.532 -0.013
SD: 0.080 0.080 0.0003
%RSD: 3.149 3.149 2.09
 
====================================================================================================
Sequence No.: 29 Autosampler Location: 
Sample ID: G1 Date Collected: 25/9/2017 16:03:10
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: G1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.745 -2.745 -0.014 16:03:12 No
 2 -2.681 -2.681 -0.014 16:03:16 No
 3 -2.541 -2.541 -0.014 16:03:20 No
 4 -2.633 -2.633 -0.014 16:03:25 No
 5 -2.584 -2.584 -0.014 16:03:29 No
Mean: -2.637 -2.637 -0.014
SD: 0.080 0.080 0.0003
%RSD: 3.024 3.024 1.97
 
====================================================================================================
Sequence No.: 30 Autosampler Location: 
Sample ID: G2 Date Collected: 25/9/2017 16:04:10
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------Replicate Data: G2
Method: Cleide 26-01-17 Page 9 Date: 25/9/2017 16:13:25 
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.793 -2.793 -0.014 16:04:11 No
 2 -2.693 -2.693 -0.014 16:04:16 No
 3 -2.782 -2.782 -0.014 16:04:20 No
 4 -2.696 -2.696 -0.014 16:04:24 No
 5 -2.670 -2.670 -0.014 16:04:28 No
Mean: -2.727 -2.727 -0.014
SD: 0.056 0.056 0.0002
%RSD: 2.066 2.066 1.33
 
====================================================================================================
Sequence No.: 31 Autosampler Location: 
Sample ID: G3 Date Collected: 25/9/2017 16:05:19
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: G3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.743 -2.743 -0.014 16:05:21 No
 2 -2.700 -2.700 -0.014 16:05:25 No
 3 -2.735 -2.735 -0.014 16:05:29 No
 4 -2.715 -2.715 -0.014 16:05:34 No
 5 -2.906 -2.906 -0.015 16:05:38 No
Mean: -2.760 -2.760 -0.014
SD: 0.083 0.083 0.0003
%RSD: 3.014 3.014 1.91
 
====================================================================================================
Sequence No.: 32 Autosampler Location: 
Sample ID: H1 Date Collected: 25/9/2017 16:06:28
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: H1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -2.787 -2.787 -0.014 16:06:29 No
 2 -2.733 -2.733 -0.014 16:06:33 No
 3 -2.885 -2.885 -0.015 16:06:38 No
 4 -3.000 -3.000 -0.015 16:06:42 No
 5 -2.918 -2.918 -0.015 16:06:46 No
Mean: -2.865 -2.865 -0.015
SD: 0.106 0.106 0.0003
%RSD: 3.701 3.701 2.34
 
====================================================================================================
Sequence No.: 33 Autosampler Location: 
Sample ID: H2 Date Collected: 25/9/2017 16:07:31
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: H2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -3.014 -3.014 -0.015 16:07:32 No
 2 -3.064 -3.064 -0.015 16:07:37 No
 3 -3.035 -3.035 -0.015 16:07:41 No
 4 -3.118 -3.118 -0.015 16:07:45 No
 5 -3.120 -3.120 -0.015 16:07:50 No
Mean: -3.070 -3.070 -0.015
SD: 0.048 0.048 0.0001
%RSD: 1.556 1.556 0.96
 
====================================================================================================
Sequence No.: 34 Autosampler Location: 
Sample ID: H3 Date Collected: 25/9/2017 16:08:28
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: H3
Method: Cleide 26-01-17 Page 10 Date: 25/9/2017 16:13:25 
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -3.128 -3.128 -0.015 16:08:29 No
 2 -3.243 -3.243 -0.016 16:08:34 No
 3 -3.191 -3.191 -0.016 16:08:38 No
 4 -3.153 -3.153 -0.015 16:08:42 No
 5 -3.277 -3.277 -0.016 16:08:47 No
Mean: -3.198 -3.198 -0.016
SD: 0.062 0.062 0.0002
%RSD: 1.927 1.927 1.17
 
====================================================================================================
Sequence No.: 35 Autosampler Location: 
Sample ID: I1 Date Collected: 25/9/2017 16:09:32
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: I1
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -3.354 -3.354 -0.016 16:09:34 No
 2 -3.204 -3.204 -0.016 16:09:38 No
 3 -3.232 -3.232 -0.016 16:09:42 No
 4 -3.441 -3.441 -0.016 16:09:46 No
 5 -3.354 -3.354 -0.016 16:09:51 No
Mean: -3.317 -3.317 -0.016
SD: 0.098 0.098 0.0003
%RSD: 2.940 2.940 1.76
 
====================================================================================================
Sequence No.: 36 Autosampler Location: 
Sample ID: I2 Date Collected: 25/9/2017 16:10:25
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: I2
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -3.418 -3.418 -0.016 16:10:26 No
 2 -3.314 -3.314 -0.016 16:10:31 No
 3 -3.482 -3.482 -0.016 16:10:35 No
 4 -3.399 -3.399 -0.016 16:10:39 No
 5 -3.316 -3.316 -0.016 16:10:44 No
Mean: -3.386 -3.386 -0.016
SD: 0.072 0.072 0.0002
%RSD: 2.113 2.113 1.25
 
====================================================================================================
Sequence No.: 37 Autosampler Location: 
Sample ID: I3 Date Collected: 25/9/2017 16:11:29
Analyst: Data Type: Original
 
----------------------------------------------------------------------------------------------------
Replicate Data: I3
Repl SampleConc StndConc BlnkCorr Time Signal
 # mg/L mg/L Signal Stored
 1 -3.611 -3.611 -0.017 16:11:31 No
 2 -3.564 -3.564 -0.017 16:11:35 No
 3 -3.663 -3.663 -0.017 16:11:39 No
 4 -3.578 -3.578 -0.017 16:11:43 No
 5 -3.591 -3.591 -0.017 16:11:48 No
Mean: -3.602 -3.602 -0.017
SD: 0.039 0.039 0.0001
%RSD: 1.074 1.074 0.62