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Metodologia do Trabalho Científico Vitor R. Coluci Faculdade de Tecnologia - UNICAMP http://www.ft.unicamp.br/vitor Visualização Científica Apresentação Científica Posters e Seminários Roteiro Motivação Ilustração: Tabelas e Figuras Softwares para elaboração de Gráficos Dicas para elaborar um bom gráfico (Exemplos) Etapa importante no trabalho científico: Divulgação e apresentação dos resultados obtidos -Revistas científicas especializadas nacionais e internacionais -Teses e Relatórios Visualização científica é o processo de representar dados científicos como imagens que podem auxiliar o entendimento dos significados dos dados. Tabelas - Figuras Motivação Ilustração Tabela Figuras Fotos Esquemas Desenhos Gráficos pronounced ion acceleration pointing in laser propagation direction which might also be connected to quasimonoe- nergetic ion emission [6] in the case of water droplets. Since the droplets are not grounded the decreasing of the charge can not be explained as in [21] by redistribution of charge supported by the mounting. The charge neutraliza- tion can be driven by the ionized surrounding background gas. The 0.14 nC charge corresponds to a lack of 9! 108 electrons. Electrons can stem from the neighbor droplets and the background gas. The electric field of the charged droplet can field-ionize the neighbor droplets as well as the background gas, which is caused by the evaporation of the droplets. Also the laser beam is quite more extended (around 100 !m) at IL ¼ 1012–1013 W=cm2 and ionizes the background gas. From pressure measurement we esti- mate the ion density of the ambient plasma to be 1012 cm#3. In an analytical approach the potential of the droplet is derived from Poisson equation with an exponen- tial screening term [22] and the electrons move in this field. Thus the traveling time of an electron along the radius of an ambient plasma sphere which contains the amount of charge for compensation of the droplet charge resembles the ‘‘discharge’’ time of the droplet. Following Ref. [23], one can calculate the hot electron temperature Th of the electrons produced by the CPA2 laser pulse: Th$mec2ð"L#1Þ, "L¼ð1þ0:7I18#2L;!mÞ1=2 withme—the electron rest mass, I18—the laser intensity in units of 1018 W=cm2 and #L;!m—the laser wavelength in !m. The number of electrons Neh which can overcome the electrostatic barrier at the rear side can be estimated by [24]: Neh $ mec24$"0rL=e20ð"L # 1Þ, e0—elementary charge, rL—scales roughly with the laser beam radius which produces an electron bunch with a similar radius. For the experiment with I18 ¼ 2 one obtains Th $ 190 keV and Neh $ 1! 109 for rL ¼ 5–8 !m which can account for a target charge of around 0.1–0.17 nC. The charge is increasing over only a few picoseconds while the hot electrons are leaving. The movement of electrons in the ambient plasma around the droplet is described by €xþ % _x ¼ #eqðxÞ TerDðx0 þ 1Þ e#ðx#x0Þ x ! 1þ 1 x " ; (1) where x ¼ r=rD is the relative coordinate concerning the radial distance r, normalized to the Debye length rD of the ambient plasma (with an initial electron temperature of Te $ 1 keV) and the relative damping rate is % ¼ ð%ei þ %plÞ=!pe incorporating the electron-ion collision %ei, the plasma wave damping rate [25,26] %pl and the plasma electron frequency !pe. Analytical solutions exist for the limits %( 1 and %) 1. We solved the equation numeri- cally for our parameters where %< 1 and %ei > %pl. The movement of electrons to the center of charge x0 deceases the droplet charge which is adapted to an effective charge FIG. 4 (color). 2D-PIC simulation [27] of a laser irradiated droplet: distribution of the electric field 220 fs after the irradia- tion peak of a 40 fs, 2! 1018 W=cm2 laser pulse. (Laser from the left.) a b FIG. 3 (color online). (a) Accumulated proton spectra (50 shots) emitted from the droplet, (b) Scan through the proton image (black line) in comparison to scans through simulated images with varying decay time &2. The shape of the experimental trace could be reproduced best with a decay time of about 50 ps. PRL 103, 135003 (2009) P HY S I CA L R EV I EW LE T T E R S week ending 25 SEPTEMBER 2009 135003-3 • • • quadlayer (QL),32 is shown schematically in Figure 1. The exponential growth observed in the ellipsometric data in Figure 1c is believed to be caused by interdiffusion of the weak polyelectrolytes (PEI and PAA) during deposition.33,34 This system has a thickness of approximately 174 nm after only six quadlayers are deposited onto silicon. Quartz crystal microbalance data confirm both the exponential growth trend observed with ellipsometry and uniform clay deposi- tion, with all clay layers containing approximately the same mass per layer (Figure 1d).35 A five QL film contains 26.2 wt % clay (Table 1), which is nearly an order of magnitude greater than most conventional bulk composites.13,14 Fur- thermore, QCM confirms the clay concentration decreases with the number of QLs deposited, which is expected because it is the polyelectrolyte pairs that are contributing to the exponential growth, rather than the clay (see Table 1). UV-vis spectroscopy reveals that a five QL film has an average light transmission of 95% across the visible light spectrum (390-750 nm), as shown in Figure 2a.36 This high level of transparency is common to LbL films containing high concentrations of well-separated clay platelets and is a key requirement for display encapsulation (Figure 2b). A transmission electronmicroscope (TEM) image of a five QL film cross section is shown in Figure 3a.37 Individual clay platelets can be seen as dark lines in this micrograph, which reveals a more open nano brick wall structure than seen recently for more traditional polymer-clay bilayer assem- blies.29 This image emphasizes the high level of clay orienta- tion, with all platelets lying parallel to the polystyrene substrate. Many individual platelets can be resolved, as well as a few intercalated stacks of platelets, suggesting a high level of clay exfoliation. A small amount of platelet edge overlap can be observed in this image. An atomic force microscopy (AFM) phase image of this five QL film’s surface (Figure 3b)38 reveals tight clay packing and a cobblestone- path-like structure, which has been reported previously in LbL clay-polymer films.28,29When taken together, the TEM and AFM images suggest that all clay platelets deposit in the film parallel to the substrate surface. Obtaining this extent of clay exfoliation and near-perfect orientation is only pos- sible with the LbL process, due to its self-assembling and self- terminating growth. Other techniques, where direct mixing of clay and polymer were used, have also achieved a good level of clay orientation16,17 but cannot achieve the same tightly packed, laminar clay layers shown here (Figure 3). Films from these “one pot” mixtures suffer from poor clay exfoliation, transparency, and barrier. During LbL deposi- tion, the negatively charged surface of MMT is electrostati- cally attracted to the positively charged film surface created FIGURE 1. Illustrations of (a)the LbL process and (b) the nano brick wall structure resulting from the alternate adsorption of PEI (blue), PAA (green), PEI, and MMT (red) onto a substrate. (c) Thickness as a function of cycles deposited on silicon wafers of (PEI/PAA)2n (0) (R2 ) 0.982) and (PEI/PAA/PEI/MMT)n (O) (R2 ) 0.998), where PEI/PAA growth is shown to emphasize the source of exponential growth in the quadlayers. (d) Mass deposited as a function of quadlayers measured by quartz crystal microbalance, where (PEI/PAA/PEI) mass deposition is denoted as filled points and MMT as unfilled points. TABLE 1. Composition, Thickness, and Oxygen Permeability of Thin Film Assemblies permeability (10-16 cm3 (STP)·cm/(cm2·s·Pa)) thin film assembly clay concn (wt %) film thickness (nm) filma,b totalb (PEI/PAA)3.5 0 48.7 0.227 16.80 2 QL 53.7 16.1 0.066 16.70 3 QL 48.6 28.3 0.002 4.79 4 QL 36.7 50.9 e0.000005 e0.001 5 QL 26.2 82.6 <0.000009 <0.001 a Film permeability was decoupled from the total permeability using a previously described method, ref 28. b The low end detection limit for an Ox Tran 2/21 L module is 0.005 cm3/(m2·day·atm). FIGURE 2. (a) Visible light transmission as a function of wavelength for a 5 QL film on a fused quartz slide. (b) Image of a 5 QL film on 179 µm PET film in front of a screen to demonstrate optical clarity for potential use with flexible displays. © XXXX American Chemical Society B DOI: 10.1021/nl103047k | Nano Lett. XXXX, xxx, 000-–000 presented remains valid. Once the applied stress is with- drawn, the strain in the CNWs is released and so is the piezoelectric field; the inductive charges in the electrode plates have to flow back. This is the process of producing an ac output current.22 For easy visualization of the calculated potential, the orientation relationship between the realistic model for the measurement (Figure 2a) and the representing cross sections (Figure 2b) at which the distribution of the potential were exhibited (Figure 2c and 2d) can be correlated by the (x, y, z) coordinate as indicated in the corresponding figures. The piezopotential inside the CNWs is rather high so that it is plotted separately in Figure 2c. Owing to the conical shape of the nanowires and the opposite c axis, the piezopotentials inside the two CNWs are opposite in sign under compressive strain, but with a small separation in the charge centers in the direction normal to the substrate surface, which is the fundamental mechanism for creating the inductive charges at the top and bottom electrodes. By adjusting the display scale of the piezopotential in the space outside of the CNWs, a 0.8 V inductive potential difference across the two elec- trodes is clearly shown (Figure 2d), which is generated by an applied compressive strain of 0.12% at the fixed end of the CNW (maximum strain). This is the driving force for the ac nanogenerator. As a verification of the conical shape of the NW being the key of the piezopotential in our design, a calculation for cylindrical nanowires23 with zero conical angle showed that there is no potential difference across the two electrodes (Figure 2e). Our calculation also predicts that the voltage across the top and bottom electrodes is ap- proximately proportional to the thickness projected density of CNWs if the total deposition is less than a monolayer (Figure 2f). FIGURE 2. Simulation of the nanogenerator. (a) Schematic model showing the setup for measuring the energy conversion. The polystyrene substrate used to hold the NG at its upper side, where the force F is applied, is not shown here for clarity of presentation. The CNWs are under compressive strain during the deformation. (b) The unit cell and model used for calculating the potential distribution across the top and bottom electrodes of the NG with the presence of a pair of CNWs, where the corresponding cross sections at which the potential distributions were exhibited are indicated by dashed lines, and the results are shown in (c, d), respectively. Owing to the large magnitude variation in the potential distribution across the cross section, we use both color grade and equal potential lines to present the local potential. The blank region close to the CNWs is the region where the calculated piezopotential is smaller than -0.4 V, beyond the range selected for the color plotting. In order to show the detail in this region, we only used equal potential lines to present it. The CNWs were positioned close to the bottom of the unit cell in (b) to ensure that they were under compressive strain once a transverse force was applied in order to match the experimental case. (e) We also calculated the potential induced by perfect cylindrical NWs (e.g., zero conical angle). The result indicated that there was no potential difference being generated at the two electrodes. Presented is the cross section output of the calculated piezopotential similar to part d. (f) Calculated potential difference between the top and bottom electrodes of a nanogenerator as a function of the thickness projected conical nanowire density. The distance between the top and bottom electrode was kept constant (5 µm). The density required for a uniform, fully packed, monolayer coverage of the substrate is ∼90000/mm2. © XXXX American Chemical Society C DOI: 10.1021/nl103203u | Nano Lett. XXXX, xxx, 000-–000 Representar dados numéricos - podem incluir alto grau de precisão (grande número de dígitos significativos) - facilitam localização de um dado. Tabelas From: http://physics.nist.gov/constants Fundamental Physical Constants — Universal constants Relative std. Quantity Symbol Value Unit uncert. ur speed of light in vacuum c, c0 299 792 458 m s�1 (exact) magnetic constant µ0 4�� 10�7 N A�2 = 12.566 370 614...� 10�7 N A�2 (exact) electric constant 1/µ0c2 �0 8.854 187 817...� 10�12 F m�1 (exact) characteristic impedance of vacuum � µ0/�0 = µ0c Z0 376.730 313 461... � (exact) Newtonian constant of gravitation G 6.674 28(67)� 10�11 m3 kg�1 s�2 1.0� 10�4 G/h¯c 6.708 81(67)� 10�39 (GeV/c2)�2 1.0� 10�4 Planck constant h 6.626 068 96(33)� 10�34 J s 5.0� 10�8 in eV s 4.135 667 33(10)� 10�15 eV s 2.5� 10�8 h/2� h¯ 1.054 571 628(53)� 10�34 J s 5.0� 10�8 in eV s 6.582 118 99(16)� 10�16 eV s 2.5� 10�8 h¯c in MeV fm 197.326 9631(49) MeV fm 2.5� 10�8 Planck mass (h¯c/G)1/2 mP 2.176 44(11)� 10�8 kg 5.0� 10�5 energy equivalent in GeV mPc2 1.220 892(61)� 1019 GeV 5.0� 10�5 Planck temperature (h¯c5/G)1/2/k TP 1.416 785(71)� 1032 K 5.0� 10�5 Planck length h¯/mPc = (h¯G/c3)1/2 lP 1.616 252(81)� 10�35 m 5.0� 10�5 Planck time lP/c = (h¯G/c5)1/2 tP 5.391 24(27)� 10�44 s 5.0� 10�5 Page 1 Partes de uma tabela http://abacus.bates.edu/~ganderso/biology/resources/writing/HTWtablefigs.html Tabela: - deve ser clara - deve ser numerada (mencionada no texto) - deve ter um legenda (entendimento sem precisar voltar ao texto principal) - deve ser necessária.... ±” “Almost Everything You Wanted to Know About Making Tables and Figures,” Department of Biology, Bates College The oak seedlings grew at temperature between 20 and 40oC; no measurable growth occurred at temperatures below 20oC or above 40oC. Magnetic walls are assumed in the symmetry planes. A mesh with 2847 tetrahedral elements was used, generating 2797 cotrees, and 456 trees. The parameter s was 104 which is enough to shift the spectrum of DC modes out of the region of analysis. Table 1 shows the results only for solenoidal modes and those obtained from the method reported by Ref. 9. The DC modes generated by (6) is not shown. However, when the proposed method is used, the first eigenvalue obtained is a physical mode. From this table, it is possible to observe that the solenoidal solutions obtained from unconstrained and constrained formulations are exactly the same. Also, these results concur with those described in Ref. 9. Finally, as described in Section 2, the matrix [K] has a problem of the singularity. Conversely, the condition number of [K0] is approximately 7 ! 106, which means that the developed method improved the conditioning of the matrix system. The second example is a circular cavity with er ¼ 30 as shown in Figure 2. The geometry of this resonator cavity is enclosed by an electric wall. The mesh used has 1397 tetrahe- dral elements, 1662 cotrees, and 393 trees, which correspond to 393 DC modes. Table 2 shows the results obtained for solenoi- dal fields. Once again, the results obtained from the uncon- strained and constrained formulations are the same. However, the constrained formulation does not show the DC modes. In this example, the condition numbers of [K0] is 7 ! 105. 5. CONCLUSION A new approach to overcome the problem of DC modes in the solutions of eigenvalue problems was presented. The method uses only the edge basis functions and the constraint condition is imposed directly on the matrix system, improving the condition- ing of the matrix system. Two different resonator cavities were analyzed to validate the formulation. In both cases, the DC modes were eliminated without affecting the solenoidal solutions. ACKNOWLEDGMENTS The authors thank the partial support of FAPESP and FAEPEX/ UNICAMP, Brazil. REFERENCES 1. J.M. Jin, The finite element method in electromagnetics, 2nd ed., Wiley, New York, 2002. 2. M.S. Gonc¸alves, H.E. Hern!andez-Figueroa, and A.C Bordonalli, Time-domain full- band method using orthogonal edge basis func- tions, IEEE Photon Technol Lett 18 (2006), 52–54. 3. J.B. Manges and Z.J. Cendes, A generalized tree-cotree gauge for magnetic field computation, IEEE Trans Magn 31 (1995), 1342–1345. 4. N.V. Venkatarayalu and J.-F. Lee, Removal of spurious DC modes in edge element solutions for modeling three-dimensional resona- tors, IEEE Trans Microwave Theory Tech 54 (2006), 3019–3025. 5. R. Wang, D.J. Riley, and J.M. Jin, Application of tree-cotree split- ting to the time- domain finite-element analysis of electromagnetic problems, IEEE Trans Antennas Propag 58 (2010), 1590–1600. 6. S.C. Lee, J.F. Lee, and R. Lee, Hierarchical vector finite elements for analyzing waveguiding structures, IEEE Trans Microwave Theory Tech 51 (2003), 1897–1905. 7. J Webb, Edge elements and what they can do for you, IEEE Trans Magn 29 (1993), 1460–1465. 8. R. Dyczij-Edlinger, G. Peng, and J.F. Lee, A fast vector-potential method using tangentially continuous vector finite elements, IEEE Trans Microwave Theory Tech 46 (1998), 863–868. 9. I. Bardi, O. Biro, and K. Preis, Finite element scheme for 3D cav- ities without spurious modes, IEEE Trans Magn 27 (1991), 4036–4039. VC 2012 Wiley Periodicals, Inc. DESIGN OF TRI-BAND MICROSTRIP BPF USING SLR AND QUARTER- WAVELENGTH SIR Hong-Wei Deng,1 Yong-Jiu Zhao,1 Yong Fu,1 Xiao-Jun Zhou,1 and Yan-Yun Liu2 1College of Electronic and Information Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; Corresponding author: hwdeng@nuaa.edu.cn 2 Institute of Command Automation, PLA University of Science and Technology, Nanjing 210007, China Received 24 April 2012 ABSTRACT: A tri-band microstrip bandpass filter (BPF) with compact size and high selectivity is presented by using the stub-loaded resonator (SLR) and quarter-wavelength stepped-impedance resonator (SIR). The TABLE 1 First Six Eigenvalues for a Resonator Cavity (m21) of Figure 1 Mode Bardi et al. [9] Unconstrained k0 (m #1) Unconstrained k0 (m #1) 1 5.397 5.331 5.331 2 7.814 7.854 7.854 3 9.916 9.879 9.879 4 10.635 10.615 10.615 5 11.600 11.569 11.569 6 12.409 12.359 12.359 Figure 2 Circular cavity filled with a dielectric of er ¼ 30 TABLE 2 First Four Eigenvalues for a Resonator Cavity (m21) of Figure 2 Mode No. Analytical Unconstrained Constrained k0 (m #1) Error (%) k0 (m #1) Error (%) TE010 87.754 88.772 1.16 88.772 1.16 TM111 132.873 132.957 0.063 132.957 0.063 TM110 139.822 140.942 0.801 140.942 0.801 TM011 144.369 144.367 0.0013 144.367 0.0013 212 MICROWAVE AND OPTICAL TECHNOLOGY LETTERS / Vol. 55, No. 1, January 2013 DOI 10.1002/mopDOI: 10.1002/mop.27256 Magnetic walls are assumed in the symmetry planes. A mesh with 2847 tetrahedral elements was used, generating 2797 cotrees,and 456 trees. The parameter s was 104 which is enough to shift the spectrum of DC modes out of the region of analysis. Table 1 shows the results only for solenoidal modes and those obtained from the method reported by Ref. 9. The DC modes generated by (6) is not shown. However, when the proposed method is used, the first eigenvalue obtained is a physical mode. From this table, it is possible to observe that the solenoidal solutions obtained from unconstrained and constrained formulations are exactly the same. Also, these results concur with those described in Ref. 9. Finally, as described in Section 2, the matrix [K] has a problem of the singularity. Conversely, the condition number of [K0] is approximately 7 ! 106, which means that the developed method improved the conditioning of the matrix system. The second example is a circular cavity with er ¼ 30 as shown in Figure 2. The geometry of this resonator cavity is enclosed by an electric wall. The mesh used has 1397 tetrahe- dral elements, 1662 cotrees, and 393 trees, which correspond to 393 DC modes. Table 2 shows the results obtained for solenoi- dal fields. Once again, the results obtained from the uncon- strained and constrained formulations are the same. However, the constrained formulation does not show the DC modes. In this example, the condition numbers of [K0] is 7 ! 105. 5. CONCLUSION A new approach to overcome the problem of DC modes in the solutions of eigenvalue problems was presented. The method uses only the edge basis functions and the constraint condition is imposed directly on the matrix system, improving the condition- ing of the matrix system. Two different resonator cavities were analyzed to validate the formulation. In both cases, the DC modes were eliminated without affecting the solenoidal solutions. ACKNOWLEDGMENTS The authors thank the partial support of FAPESP and FAEPEX/ UNICAMP, Brazil. REFERENCES 1. J.M. Jin, The finite element method in electromagnetics, 2nd ed., Wiley, New York, 2002. 2. M.S. Gonc¸alves, H.E. Hern!andez-Figueroa, and A.C Bordonalli, Time-domain full- band method using orthogonal edge basis func- tions, IEEE Photon Technol Lett 18 (2006), 52–54. 3. J.B. Manges and Z.J. Cendes, A generalized tree-cotree gauge for magnetic field computation, IEEE Trans Magn 31 (1995), 1342–1345. 4. N.V. Venkatarayalu and J.-F. Lee, Removal of spurious DC modes in edge element solutions for modeling three-dimensional resona- tors, IEEE Trans Microwave Theory Tech 54 (2006), 3019–3025. 5. R. Wang, D.J. Riley, and J.M. Jin, Application of tree-cotree split- ting to the time- domain finite-element analysis of electromagnetic problems, IEEE Trans Antennas Propag 58 (2010), 1590–1600. 6. S.C. Lee, J.F. Lee, and R. Lee, Hierarchical vector finite elements for analyzing waveguiding structures, IEEE Trans Microwave Theory Tech 51 (2003), 1897–1905. 7. J Webb, Edge elements and what they can do for you, IEEE Trans Magn 29 (1993), 1460–1465. 8. R. Dyczij-Edlinger, G. Peng, and J.F. Lee, A fast vector-potential method using tangentially continuous vector finite elements, IEEE Trans Microwave Theory Tech 46 (1998), 863–868. 9. I. Bardi, O. Biro, and K. Preis, Finite element scheme for 3D cav- ities without spurious modes, IEEE Trans Magn 27 (1991), 4036–4039. VC 2012 Wiley Periodicals, Inc. DESIGN OF TRI-BAND MICROSTRIP BPF USING SLR AND QUARTER- WAVELENGTH SIR Hong-Wei Deng,1 Yong-Jiu Zhao,1 Yong Fu,1 Xiao-Jun Zhou,1 and Yan-Yun Liu2 1College of Electronic and Information Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China; Corresponding author: hwdeng@nuaa.edu.cn 2 Institute of Command Automation, PLA University of Science and Technology, Nanjing 210007, China Received 24 April 2012 ABSTRACT: A tri-band microstrip bandpass filter (BPF) with compact size and high selectivity is presented by using the stub-loaded resonator (SLR) and quarter-wavelength stepped-impedance resonator (SIR). The TABLE 1 First Six Eigenvalues for a Resonator Cavity (m21) of Figure 1 Mode Bardi et al. [9] Unconstrained k0 (m #1) Unconstrained k0 (m #1) 1 5.397 5.331 5.331 2 7.814 7.854 7.854 3 9.916 9.879 9.879 4 10.635 10.615 10.615 5 11.600 11.569 11.569 6 12.409 12.359 12.359 Figure 2 Circular cavity filled with a dielectric of er ¼ 30 TABLE 2 First Four Eigenvalues for a Resonator Cavity (m21) of Figure 2 Mode No. Analytical Unconstrained Constrained k0 (m #1) Error (%) k0 (m #1) Error (%) TE010 87.754 88.772 1.16 88.772 1.16 TM111 132.873 132.957 0.063 132.957 0.063 TM110 139.822 140.942 0.801 140.942 0.801 TM011 144.369 144.367 0.0013 144.367 0.0013 212 MICROWAVE AND OPTICAL TECHNOLOGY LETTERS / Vol. 55, No. 1, January 2013 DOI 10.1002/mop Fotos: mostram um alto grau de detalhe Figuras tory. Based on the launch speeds we used, the two cameras recorded the ball’s trajectory during about one-third of its time in the air. Both high-speed cameras recorded at a rate of 1000 frames/s. There are more elaborate and expensive experimental set- ups available, such as the HAWK-EYE system,28 which is used in cricket, tennis, and, more recently, snooker. Our budget allowed the use of two quality high-speed cameras !"$2500 per camera#. More sophisticated systems, which employ as many as six high-speed cameras for full three-dimensional data acquisition, are an order of magnitude more expensive than our system. Such systems are capable of tracking pro- jected objects, although determining accurate rotation rates is still a challenge. We also used markers on the ground to note the range of each launched ball. Based on visual observation of the land- ing positions, we estimate our range error to be no more than !5 cm. CINE VIEWER29 was used to convert a cine to AVI format. We did not notice any frame loss, a problem sometimes found when converting to AVI. Our software was used to track the ball and to obtain Cartesian coordinates of the ball’s center of mass.30 Figure 3 shows a sample of the data taken from camera 1. Figure 4 shows data taken from camera 2 of the launch shown in Fig. 3. Once the data points were loaded into a file, the initial launch condition was obtained. The launch position is deter- mined by measuring the height of the ball launcher’s exit. The components of the initial velocity were determined us- ing Richardson extrapolation,31,32 which gives, among other results, a forward-difference expression for the first deriva- tive using three points. If we want the derivative of a func- tion f!t# at t0 and we know the value of f!t# at t0, t1, and t2, where t1= t0+"t and t2= t0+2"t for a step size "t, then the Richardson extrapolation gives for the first derivative at t0 f!!t0# $ − 3f!t0# + 4f!t1# − f!t2# 2"t , !4# where the error is of order !"t#2. The spin rate was determined by following a given point on the ball as the ball turned either a half turn !for slow spins# or a full turn !for fast spins#. We achieved initial spin rates in the range from no spin to about 180 rad/s !more than 1700 rpm#, though most tests were carried out for spin rates less than 125 rad/s. III. FORCES ON BALL The forces on projectiles moving through air have been discussed in many articles33 and books.34 Figure 5 shows the various forces on the ball. We assume the soccer ball’s tra- jectory to be close enough to the surface of the Earth so that the gravitational force on the ball, mg! , is constant. The mass of the ball is m=0.424 kg. The air exerts a force on the soccer ball. The contribution to the air’s force from buoyancy is small !"0.07 N# and is ignored. A scale used to determine weight will have that small force subtracted off anyway. The major contributions Fig. 1. Ball launcher used for the trajectory experiments. Note the ball emergingfrom the launcher and the location of camera 1 on the right side of the photo. Fig. 2. A not-to-scale sketch of the experimental setup. Camera 1, about 1.5 m from the plane of the trajectory, records the launch of the soccer ball. Camera 2, about 13 m from the plane of the trajectory, records a portion of the trajectory near the apex of the flight. The z axis !not shown# points out of the page. Fig. 3. Data from camera 1 for a launch with no spin. The centers of the circles denote the ball’s center of mass in 0.005 s intervals. The ball was launched with speed of v0$18 m /s at an angle of #0$22° from the horizontal. Fig. 4. Data from camera 2 for the no-spin launch in Fig. 3. Each circle’s center notes the ball’s center of mass in 0.010 s intervals. For more accurate results we zoom the image to four times what is shown. The ball landed 21.9 m from the launcher’s base. 1021 1021Am. J. Phys., Vol. 77, No. 11, November 2009 John Eric Goff and Matt J. Carré Desenhos: grau menor de detalhes (para enfatizar certos aspectos) permitem capturar aspectos que não podem ser fotografados Figuras http://agetec.com.br/news/4/114/Aplicacao-do-processo-de-flotacao-para-separacao-de-fases-em-ETA/ http://www.portalsaofrancisco.com.br/alfa/celula-vegetal/imagens/celula-vegetal-7.gif Figuras Ronaldo Giro; Márcio Cyrillo; Douglas Soares Galvão Mat. Res. vol.6 no.4 São Carlos Oct./Dec. 2003 doi: 10.1590/S1516-14392003000400017 Esquemas: Esquemas (Figuras em geral): Camera Control Terminal Printer ComputerDigitizer Missile Electro- mechanical interface The testing hardware of the missile shown in Figure 11-6 has five main components: camera, digitizer, computer, I/O interface, and mechanical interface. Commands are generated by the computer and then passed through the I/O interface to the mechanical interface where the keyboard of the ICU is operated. The display of the ICU is read with a television camera and digitized. This information is the manipulated by the computer to direct the next command to the I/O interface. -Precisão -Clareza -Familiaridade -Fluidez Esquema confuso... Esquemas: Camera Computer Digitizer Missile Electro- mechanical interface Our system for testing the safety devices of the missile consists of four main parts: computer, camera, digitizer, and electromechanical interface to the missile. In this system, shown in Figure 11-6, the computer generates test commands to the missile through the electromechanical interface. The test results are read with a television camera and then digitized. The computer receives the information from the digitizer and then directs the next test command. Figure 11-6. System for testing the safety devices of missile. Esquema OK... Gráficos: - comparar teoria e experimento; - mostrar relações entre variáveis - evidenciar tendências O gráfico deve ser bem feito para ser bem interpretado e efetivamente útil. Figuras http://www.astro.ucla.edu/~wright/sne_cosmology.html ment and van der Waals forces along incidental points (and lines) of contact. These observa- tions enable prediction of the actuator proper- ties that are ultimately obtainable for non- bundled nanotubes, which have extraordinarily high surface area and mechanical properties (8). The concept of using either nanotube sheets or single nanotubes as actuators, and the effect of nanotube bundling, are schematically illustrated in Fig. 2. The commercially obtained nanotubes were made by the dual pulsed-laser vaporization method and purified by a published method that involves nitric acid reflux, cycles of washing and centrifugation, and cross-flow filtration (4, 9). Materials made by this method consist of hexagonally packed bundles of carbon nano- tubes that have diameters of 12 to 14 Å, an intertube separation within a bundle of!17 Å, an average bundle diameter of !100 Å, and lengths of many micrometers (4, 10). The nano- tube sheets were formed by vacuum filtration of a nanotube suspension on a poly(tetrafluoreth- ylene) filter, and the dried nanotube sheets were peeled from the filter (4, 9). These freestanding sheets (composed of highly entangled nano- tube bundles) were used as they were ob- tained, without any effort to optimize the mechanical properties, surface area, or elec- trical conductivity that are important for the actuator application. The electrochemical charge injection pro- cess was characterized by measurement of the gravimetric capacitance (CG) of the nanotube paper in various electrolytes [all potentials are versus a saturated calomel electrode (SCE)].CG was derived from the slope of specific current versus voltage scan rate in a cell containing nanotube paper for both a working electrode and a counterelectrode. After a few cycles to ensure the maximum degree of electrode wet- ting, the measured CG increased up to about 15 F/g for aqueous solutions of both 1MNaCl and 38% by weight H2SO4. Similar CGs were ob- served for 1 M LiClO4 in acetonitrile (12 to 17 F/g) or in propylene carbonate (13 to 14 F/g), and a higher CG was observed for a 5 M aqueous KOH solution (30 F/g), which readily wet the nanotube paper. These measurements and estimates of the available surface area suggest that double-layer charge injection for the nanotube bundles is similar to that for the basal plane of graphite. The gravimetric surface area of the nanotube paper (AG) measured by the Brunauer-Emmett- Teller (BET) method is about 285 m2/g (11); this value is near the 300 m2/g surface area of 100 Å diameter cylinders having the crystallo- graphically derived bundle density of 1.33 g/cm3 (10), which suggests that the N2 in the BET measurement does not access significant surface area in the space between nanotubes in a bundle. An areal capacitance (CA) of 4 to 10 "F/cm2 results for the above range of ob- served gravimetric capacitances and an AG of 300 m2/g. This value is in the approxi- mate range of measured CAs for the basal plane of graphite (12), which has a mini- mum at !3 "F/cm2 (for either 0.9 M aque- ous NaF or 0.2 M tetrapropylammonium tetrafluoride solution in acetonitrile). Our first demonstration of a carbon nano- tube actuator was surprisingly simple to pro- duce. Similar to a design for a polyaniline con- ducting polymer actuator (3) (Fig. 3), this ac- Fig. 1. Experimentally derived changes in basal plane strain as a function of nominal charge derived from data (6) for graphite intercalation compounds. A B Fig. 2. Schematic illustration of charge injec- tion in a nanotube-based electromechanical ac- tuator and the effect of nanotube bundling. (A) An applied potential injects charge of opposite sign in the two pictured nanotube electrodes, which are in a liquid or solid electrolyte (blue background). These indicated charges in each electrode are completely balanced by ions from the electrolyte (denoted by the charged spheres on each nanotube cylinder). The pictured single nanotube electrodes represent an arbitrary number of nanotubes in each electrode that mechan- ically and electrically act in parallel. Depending on the potential and the relative number of nanotubes in each electrode, the opposite electrodes can provide either in-phase or out-of-phase mechanical deformations. (B) Charge injection at the surface of a nanotube bundle is illustrated, which is balanced by the pictured surface layer of electrolyte cations. Although penetration of electrolyte and gases into interstitial sites and nanotube cores might occur for the investigated bundled nanotubes, this has no noticeable effect on the observed BET surface area (11) or the measured electrode capacitance. Fig. 3. Schematic edge- view of a cantilever-based actuator operated in aque- ous NaCl, which consists of two strips of SWNTs (shad- ed)that are laminated to- gether with an intermedi- ate layer of double-sided Scotch tape (white). The Na# and Cl– ions in the nanotube sheets represent ions in the double layer at the nanotube bundle surfaces, which are com- pensated by the indicated charges that are injected into the nanotube bundles. The equality between the lengths of the two nano- tube sheets (center) is dis- rupted when a voltage is applied, causing the indi- cated actuator displace- ments to the left or right. The possible existence of a small amount of double-layer charge before the application of a voltage is ignored. R E P O R T S www.sciencemag.org SCIENCE VOL 284 21 MAY 1999 1341 o n S e p te m b e r 2 8 , 2 0 0 9 w w w .s c ie n c e m a g .o rg D o w n lo a d e d f ro m Carbon Nanotube Actuators Ray H. Baughman, et al Science 21 May 1999 284: 1340-1344 [DOI: 10.1126/science.284.5418.1340] • • • • • • Partes de um gráfico Softwares 1) SciGraphica 2) LabPlot http://labplot.sourceforge.net/ 3) Veusz (Linux,Windows, MacOS) http://home.gna.org/veusz/ 4) Gnuplot (Linux,Windows, MacOS) http://www.gnuplot.info/ 5) Xmgrace (Linux, Windows) http://plasma-gate.weizmann.ac.il/Grace/ 6) PSTricks (http://tug.org/PSTricks/main.cgi/) Lista http://en.wikipedia.org/wiki/List_of_graphing_software SciGraphica SciGraphica Scigraphica LabPlot LabPlot Gnuplot Command-line driven interactive data and function plotting utility (UNIX, IBM OS/2, MS Windows, DOS, Macintosh, VMS, Atari, etc). 2D and 3D plots. Lines, points, boxes, contours, vector fields, surfaces, and various associated text. Different types of output: interactive screen terminals (with mouse and hotkey functionality), Direct output to pen plotters or modern printers, Output to many file formats (eps, fig, jpeg, LaTeX, metafont, pbm, pdf, png, postscript, svg, ...). Gnuplot # set terminal png transparent nocrop enhanced font arial 8 size 420,320 # set output 'simple.1.png' set key inside left top vertical Right noreverse enhanced autotitles box linetype -1 linewidth 1.000 set samples 50, 50 plot [-10:10] sin(x),atan(x),cos(atan(x)) $ gnuplot s1.gnu # set terminal png transparent nocrop enhanced font arial 8 size 420,320 # set output 'contours.1.png' set view 60, 30, 0.85, 1.1 set samples 20, 20 set isosamples 21, 21 set contour base set title "3D gnuplot demo - contour plot" set xlabel "X axis" set ylabel "Y axis" set zlabel "Z axis" set zlabel offset character 1, 0, 0 font "" textcolor lt -1 norotate splot x*y Xmgrace Xmgrace Xmgrace Dicas para a preparação de um bom gráfico Guia para Física Experimental: Caderno de Laboratório, Gráficos e Erros Carlos H. de Brito Cruz, Hugo L. Fragnito, Ivan F. da Costa e Bernardo de A. Mello http://www.ifi.unicamp.br/~brito/apost.html Dicas para a preparação de um bom gráfico Um gráfico bem feito é talvez a melhor forma de apresentar dados Informação do que será transmitido - argumentação para o que está se querendo demonstrar Ajuda visual para sua argumentação e para que o leitor entenda rapidamente o que você está querendo apresentar/demonstrar Vários parâmetros: Escalas/Posição dos dados, Cores, Tamanho de Fontes, Tamanho de símbolos, etc Experiência, bom senso, ... Dicas 1. Título: breve descrição do que trata o gráfico; 2. Uma legenda para cada eixo indicando que valores estão sendo ali colocados, qual a sua unidade; 3. Uma escala para cada eixo: (a) usando valores com intervalos regulares entre si (de 2 em 2, e não de 7.7 em 7.7); (b) com valores fáceis de serem lidos, como múltiplos inteiros por exemplo; (c) os dois eixos não precisam ter a mesma origem e nem tão pouco a mesma escala numérica; Dicas Evite “ligar os pontos”. Somente deverá ser usada uma curva entre os pontos quando for útil apresentar um guia para os olhos ou quando um modelo for comparado ou a justado aos pontos experimentais. Em ambos os casos, o procedimento, modelo ou utilidade da curva deve ser mostrada no texto e a curva claramente identificada. Quando conectar pontos: Medidas/Dados obtidos da mesma fonte e depender do ponto anterior (Ex.: Evolução do comprimento de um bebê) Quando NÃO conectar pontos: Medidas/Dados obtidos de maneira independente. (Ex.: Média do preço de memória de computadores durante o ano) Curva = melhor ajuste aos pontos (regressão linear, polinomial, etc...) Dicas 4. Se forem usadas abreviações no gráfico, elas devem ser explicadas no próprio gráfico ou em algum lugar do texto; 5. Os valores dos pontos nunca devem ser colocados no gráfico (tabelas). Destaque (evite carregar de informações o gráfico, somente indicando o ponto e deixando as explicações para o texto.) 6. Os pontos das medidas deverão aparecer, quando cabíveis, com suas respectivas barras de erro. Fonte: Apostila Prof. Varlei Rodrigues, Instituto de Física - UNICAMP Física Experimental: Caderno de Laboratório, Gráficos, Medidas e Erros 7 ser sempre o conceito de que um gráfico é uma ajuda visual para a sua argumentação e para que o leitor entenda rapidamente as evidências experimentais. Os gráficos são figuras e você deve escolher o tamanho das figuras de modo que caibam na folha de papel do seu texto (seja este no seu caderno de laboratório, relatório ou artigo), ocupando não mais que a metade da folha. Isto não é um critério estético, é um critério de eficácia da apresentação baseada no fato de que dificilmente alguém consegue focalizar os olhos numa área maior a uns 30 cm dos seus olhos. p o s iç ã o , x ( c m ) Fig. 2.1. Exemplo de gráfico bem feito. A Figura 2.1 mostra um gráfico eficiente para mostrar que, dentro do erro experimental, os dados seguem um determinado modelo teórico. Gráfico Bom Física Experimental: Caderno de Laboratório, Gráficos, Medidas e Erros 8 Fig. 2.2. Exemplos de gráficos mal feitos. Os mesmos dados experimentais da Fig. 2.1 estão representados novamente nos quatro gráficos da Figura 2.2 para ilustrar defeitos típicos de alunos inexperientes. O tamanho dos pontos deve ser tal que cada ponto seja bem visível; nem muito pequeno como no gráfico 1 nem exagerado como no gráfico 2, onde o tamanho do símbolo é maior que a barra de erro para a maioria dos pontos. No gráfico 2, os números das escalas são difíceis de ler. No gráfico 3 as escalas foram mal escolhidas,desaproveitando a área; o fator 1/70 e os números das marcas da escala horizontal dificultam a leitura. No gráfico 4 a escala horizontal não deve ser indicada com os valores individuais dos pontos. 2.3 Determinação dos coeficientes de uma reta É muito freqüente em física experimental o problema de determinar os estimadores a e b dos coeficientes α e β, respectivamente, que melhor representam a relação linear entre duas variáveis aleatórias X e Y: Y = αX + β, [2.1] a partir de um conjunto de pares de valores medidos (yi,xi), i = 1,.., N. Este problema é considerado em vários livros texto (veja por exemplo as refs. 1 e 2) e reproduziremos aqui os resultados mais importantes. É preciso antes observar a validade das fórmulas. Os alunos tendem a utilizar as fórmulas de ajuste por mínimos quadrados ou as de regressão linear sem Gráficos Ruins Gráficos Ruins Não tão bom Melhor ! (limpo, claro) Exemplos de gráficos publicados ment and van der Waals forces along incidental points (and lines) of contact. These observa- tions enable prediction of the actuator proper- ties that are ultimately obtainable for non- bundled nanotubes, which have extraordinarily high surface area and mechanical properties (8). The concept of using either nanotube sheets or single nanotubes as actuators, and the effect of nanotube bundling, are schematically illustrated in Fig. 2. The commercially obtained nanotubes were made by the dual pulsed-laser vaporization method and purified by a published method that involves nitric acid reflux, cycles of washing and centrifugation, and cross-flow filtration (4, 9). Materials made by this method consist of hexagonally packed bundles of carbon nano- tubes that have diameters of 12 to 14 Å, an intertube separation within a bundle of!17 Å, an average bundle diameter of !100 Å, and lengths of many micrometers (4, 10). The nano- tube sheets were formed by vacuum filtration of a nanotube suspension on a poly(tetrafluoreth- ylene) filter, and the dried nanotube sheets were peeled from the filter (4, 9). These freestanding sheets (composed of highly entangled nano- tube bundles) were used as they were ob- tained, without any effort to optimize the mechanical properties, surface area, or elec- trical conductivity that are important for the actuator application. The electrochemical charge injection pro- cess was characterized by measurement of the gravimetric capacitance (CG) of the nanotube paper in various electrolytes [all potentials are versus a saturated calomel electrode (SCE)].CG was derived from the slope of specific current versus voltage scan rate in a cell containing nanotube paper for both a working electrode and a counterelectrode. After a few cycles to ensure the maximum degree of electrode wet- ting, the measured CG increased up to about 15 F/g for aqueous solutions of both 1MNaCl and 38% by weight H2SO4. Similar CGs were ob- served for 1 M LiClO4 in acetonitrile (12 to 17 F/g) or in propylene carbonate (13 to 14 F/g), and a higher CG was observed for a 5 M aqueous KOH solution (30 F/g), which readily wet the nanotube paper. These measurements and estimates of the available surface area suggest that double-layer charge injection for the nanotube bundles is similar to that for the basal plane of graphite. The gravimetric surface area of the nanotube paper (AG) measured by the Brunauer-Emmett- Teller (BET) method is about 285 m2/g (11); this value is near the 300 m2/g surface area of 100 Å diameter cylinders having the crystallo- graphically derived bundle density of 1.33 g/cm3 (10), which suggests that the N2 in the BET measurement does not access significant surface area in the space between nanotubes in a bundle. An areal capacitance (CA) of 4 to 10 "F/cm2 results for the above range of ob- served gravimetric capacitances and an AG of 300 m2/g. This value is in the approxi- mate range of measured CAs for the basal plane of graphite (12), which has a mini- mum at !3 "F/cm2 (for either 0.9 M aque- ous NaF or 0.2 M tetrapropylammonium tetrafluoride solution in acetonitrile). Our first demonstration of a carbon nano- tube actuator was surprisingly simple to pro- duce. Similar to a design for a polyaniline con- ducting polymer actuator (3) (Fig. 3), this ac- Fig. 1. Experimentally derived changes in basal plane strain as a function of nominal charge derived from data (6) for graphite intercalation compounds. A B Fig. 2. Schematic illustration of charge injec- tion in a nanotube-based electromechanical ac- tuator and the effect of nanotube bundling. (A) An applied potential injects charge of opposite sign in the two pictured nanotube electrodes, which are in a liquid or solid electrolyte (blue background). These indicated charges in each electrode are completely balanced by ions from the electrolyte (denoted by the charged spheres on each nanotube cylinder). The pictured single nanotube electrodes represent an arbitrary number of nanotubes in each electrode that mechan- ically and electrically act in parallel. Depending on the potential and the relative number of nanotubes in each electrode, the opposite electrodes can provide either in-phase or out-of-phase mechanical deformations. (B) Charge injection at the surface of a nanotube bundle is illustrated, which is balanced by the pictured surface layer of electrolyte cations. Although penetration of electrolyte and gases into interstitial sites and nanotube cores might occur for the investigated bundled nanotubes, this has no noticeable effect on the observed BET surface area (11) or the measured electrode capacitance. Fig. 3. Schematic edge- view of a cantilever-based actuator operated in aque- ous NaCl, which consists of two strips of SWNTs (shad- ed) that are laminated to- gether with an intermedi- ate layer of double-sided Scotch tape (white). The Na# and Cl– ions in the nanotube sheets represent ions in the double layer at the nanotube bundle surfaces, which are com- pensated by the indicated charges that are injected into the nanotube bundles. The equality between the lengths of the two nano- tube sheets (center) is dis- rupted when a voltage is applied, causing the indi- cated actuator displace- ments to the left or right. The possible existence of a small amount of double-layer charge before the application of a voltage is ignored. R E P O R T S www.sciencemag.org SCIENCE VOL 284 21 MAY 1999 1341 o n S e p te m b e r 2 8 , 2 0 0 9 w w w .s c ie n c e m a g .o rg D o w n lo a d e d f ro m Carbon Nanotube Actuators Ray H. Baughman, et al Science 21 May 1999 284: 1340-1344 [DOI: 10.1126/science.284.5418.1340] Holocene Glacier Fluctuations in the Peruvian Andes Indicate Northern Climate Linkages Joseph M. Licciardi, et al. Science Vol. 325. no. 5948, pp. 1677 - 1679 DOI: 10.1126/science.1175010 [Fig. 2(a)] are assigned to cyclotron resonance transitions between adjacent LLs (j!nj ¼ 1) with energies: En ¼ signðnÞ~c ffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi2e@Bjnjp ¼ signðnÞE1 ffiffiffiffiffiffiffiffiffiffiBjnjp [8,9], characteristic of massless Dirac fermions in graphene sheets with an effective Fermi velocity ~c. This velocity is the only adjust- able parameter required to match the energies of the ob- served and calculated CR transitions. A best match is found for ~c ¼ ð1:00$ 0:02Þ % 106 m & s'1 in fair agreement with values found in multilayer epitaxial graphene [10,11] or exfoliated graphene on Si=SiO2 substrate [12– 14]. As can be seen from Figs. 2(b) and 2(c), the multimode character of the measured spectra is directly related to thermal distribution of carriers among different LLs. The intensity of a given transition is proportional to the differ- ence in thermal occupation of the involved LLs.Roughly speaking, the strongest transitions imply LLs in the vicinity of the Fermi level, which fixes EF at around 6–7 meV from the Dirac point. To reproduce the experimental data, we assume the absorption strength is proportional to the longitudinal con- ductivity of the system: !xxð!;BÞ /ð B=!Þ X m;n Mm;n fn ' fm Em ' En ' ð@!þ i"Þ ; where fn is the occupation of the n-th LL, and Mm;n ¼ #$jmj;jnj$1 with# ¼ 2 for n orm equal to 0, otherwise# ¼ 1 [10,15]. The calculated traces in Fig. 3 have been drawn taking " ¼ 35 %eV for the line broadening, ~c ¼ 1:00% 106 m & s'1 and EF ¼ 6:5 meV. To directly simulate the measured traces, the derivative of the absorption with respect to the magnetic field has been calculated taking account of the field modulation !B ¼ 0:5 mT used in the experiment. In spite of its simplicity, our model is more than in a qualitative agreement with our experimental data, see Fig. 3. The calculation fairly well reproduces the experimental trends: the multimode character of the spec- tra, the intensity distribution among the lines, as well as its evolution with temperature; and it allows us to estimate the characteristic broadening of the CR transitions. Our modeling could be further improved but at the expense of additional complexity which we want to avoid here. Assuming magnetic-field and/or LL index depen- dence of the broadening parameter " and taking into account the possible fluctuation of the Fermi level within -10 -5 0 5 10 15 20 25 30 -10 -5 0 5 10 15 -5 0 5 10 0.0 0.5 1.0 -5 0 5 10 (b) -2 00 -2 T = 25 KL n −> L n+1 Magnetic Field (mT) (a) 65 (c) De riv at ive of ab so rp tio n (ar b. u . ) -1 n=1 L0 L6 L1 L -1 L6 L3 L2 L -2 L -1 L1 432 1 Microwave energy = Magnetic Field (mT) La n da u Le ve l E n er gy (m eV ) 1.171 meV -1 L0 Distribution T = 25 K Fermi-Dirac En er gy (m eV ) EF= 6.5 meV FIG. 2 (color online). Magneto-absorption spectrum (after re- moving a weak linear background seen in the raw data of Fig. 1) measured at T¼25K and microwave frequency @!¼ 1:171meV (a) in comparison with the LL fan chart (b), where the observed cyclotron resonance (CR) transitions are shown by arrows. The occupation of individual LLs is given by the Fermi-Dirac distribution plotted in the part (c). For simplicity, we considered only n-type doping with EF ¼ 6:5 meV. The dashed lines show positions of resonances assuming ~c ¼ 1:00% 106 m & s'1. -100 -80 -60 -40 -20 0 20 40 60 80 100 Decoupled graphene Electrons in hω c (3N+1) N = 7 6 5 4 7 6 5 7.5 K Magnetic Field (mT) 1.171 meV 10 K 15 K 20 K 25 K 30 K 35 K 40 K T = 50 K D er iv a tiv e o f A bs o rp tio n (ar b. u . ) 4 bulk graphite Microwave energy FIG. 1 (color online). Magneto-absorption spectra (detected with field modulation technique) of natural graphite specimen taken in the temperature interval 7.5–50 K at fixed microwave energy @! ¼ 1:171 meV. The response of low electron concen- tration graphene layers decoupled from bulk graphite is seen within the yellow highlighted area. High CR harmonics of K point electrons in bulk graphite [21], with basic CR frequency !c corresponding to the effective mass m ¼ 0:054m0 [20] are shown by numbered arrows. The origin of features denoted by stars is discussed in the text. PRL 103, 136403 (2009) P HY S I CA L R EV I EW LE T T E R S week ending 25 SEPTEMBER 2009 136403-2 [Fig. 2(a)] are assigned to cyclotron resonance transitions between adjacent LLs (j!nj ¼ 1) with energies: En ¼ signðnÞ~c ffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi2e@Bjnjp ¼ signðnÞE1 ffiffiffiffiffiffiffiffiffiffiBjnjp [8,9], characteristic of massless Dirac fermions in graphene sheets with an effective Fermi velocity ~c. This velocity is the only adjust- able parameter required to match the energies of the ob- served and calculated CR transitions. A best match is found for ~c ¼ ð1:00$ 0:02Þ % 106 m & s'1 in fair agreement with values found in multilayer epitaxial graphene [10,11] or exfoliated graphene on Si=SiO2 substrate [12– 14]. As can be seen from Figs. 2(b) and 2(c), the multimode character of the measured spectra is directly related to thermal distribution of carriers among different LLs. The intensity of a given transition is proportional to the differ- ence in thermal occupation of the involved LLs. Roughly speaking, the strongest transitions imply LLs in the vicinity of the Fermi level, which fixes EF at around 6–7 meV from the Dirac point. To reproduce the experimental data, we assume the absorption strength is proportional to the longitudinal con- ductivity of the system: !xxð!;BÞ /ð B=!Þ X m;n Mm;n fn ' fm Em ' En ' ð@!þ i"Þ ; where fn is the occupation of the n-th LL, and Mm;n ¼ #$jmj;jnj$1 with# ¼ 2 for n orm equal to 0, otherwise# ¼ 1 [10,15]. The calculated traces in Fig. 3 have been drawn taking " ¼ 35 %eV for the line broadening, ~c ¼ 1:00% 106 m & s'1 and EF ¼ 6:5 meV. To directly simulate the measured traces, the derivative of the absorption with respect to the magnetic field has been calculated taking account of the field modulation !B ¼ 0:5 mT used in the experiment. In spite of its simplicity, our model is more than in a qualitative agreement with our experimental data, see Fig. 3. The calculation fairly well reproduces the experimental trends: the multimode character of the spec- tra, the intensity distribution among the lines, as well as its evolution with temperature; and it allows us to estimate the characteristic broadening of the CR transitions. Our modeling could be further improved but at the expense of additional complexity which we want to avoid here. Assuming magnetic-field and/or LL index depen- dence of the broadening parameter " and taking into account the possible fluctuation of the Fermi level within -10 -5 0 5 10 15 20 25 30 -10 -5 0 5 10 15 -5 0 5 10 0.0 0.5 1.0 -5 0 5 10 (b) -2 00 -2 T = 25 KL n −> L n+1 Magnetic Field (mT) (a) 65 (c) De riv at ive of ab so rp tio n (ar b. u . ) -1 n=1 L0 L6 L1 L -1 L6 L3 L2 L -2 L -1 L1 432 1 Microwave energy = Magnetic Field (mT) La n da u Le ve l E n er gy (m eV ) 1.171 meV -1 L0 Distribution T = 25 K Fermi-Dirac En er gy (m eV ) EF= 6.5 meV FIG. 2 (color online). Magneto-absorption spectrum (after re- moving a weak linear background seen in the raw data of Fig. 1) measured at T¼25K and microwave frequency @!¼ 1:171meV (a) in comparison with the LL fan chart (b), where the observed cyclotron resonance (CR) transitions are shown by arrows. The occupation of individual LLs is given by the Fermi-Dirac distribution plotted in the part (c). For simplicity, we considered only n-type doping with EF ¼ 6:5 meV. The dashed lines show positions of resonances assuming ~c ¼ 1:00% 106 m & s'1. -100 -80 -60 -40 -20 0 20 40 60 80 100 Decoupled graphene Electrons in hω c (3N+1) N = 7 6 5 4 7 6 5 7.5 K Magnetic Field (mT) 1.171 meV 10 K 15 K 20 K 25 K 30 K 35 K 40 K T = 50 K D er iv a tiv e o f A bs o rp tio n (ar b. u . ) 4 bulk graphite Microwave energy FIG. 1 (color online). Magneto-absorption spectra (detected with field modulation technique) of natural graphite specimen taken in the temperature interval 7.5–50 K at fixed microwave energy @! ¼ 1:171 meV. The response of lowelectron concen- tration graphene layers decoupled from bulk graphite is seen within the yellow highlighted area. High CR harmonics of K point electrons in bulk graphite [21], with basic CR frequency !c corresponding to the effective mass m ¼ 0:054m0 [20] are shown by numbered arrows. The origin of features denoted by stars is discussed in the text. PRL 103, 136403 (2009) P HY S I CA L R EV I EW LE T T E R S week ending 25 SEPTEMBER 2009 136403-2 How Perfect Can Graphene Be? P. Neugebauer, M. Orlita, C. Faugeras, A.-L. Barra, and M. Potemski, PRL 103, 136403 (2009) Apresentação Científica Posters e Seminários Etapa importante no trabalho científico: Divulgação e apresentação dos resultados obtidos -Revistas científicas especializadas nacionais e internacionais -Teses e Relatórios -Posters e Seminários Motivação Poster Científico Posters: Apresentar o trabalho para uma audiência em movimento... (distrações, ....) Posters: Propaganda do seu trabalho Posters: Qual a audiência? Especialistas, público leigo,... Não são artigos/relatórios colocados num quadro Deve ter menos informações que o artigo (informação essencial) Concentre-se em uma única mensagem (ou poucas ...) Menos é Mais !!! Posters: Tipografia: -Usar fontes que permita a leitura de longe -Usar fontes do tipo Sans Serif (Arial, etc..) Sans Serif vs Serif - Evite usar bloco de letras maiúsculas 1-nitropyrene (1-NP), which is mutagenic and carcionogenic, is one of the most abundant nitro polycyclic aromatic hydrocarbon (nitro-PAH) in the environment. Strategies to remediate organic pollutants have been developed and nanomaterials like carbon nanotubes (CNT) are one of them. They present high specific surface area, an useful property for molecule adsorption. Nitric acid treatment can introduce oxygenated groups (e.g. carboxylic acids) on the CNT surfaces increasing water solubility but decreasing the ability of CNT to interact with organic molecules. We used samples of acid-treated MWCNT to investigate the ability of CNT to adsorb 1-NP. Diferent doses of well characterized CNTs were tested against diferent doses of 1-NP and the detection of the non-adsorbed 1-NP was performed with the Salmonella/ microsome mutagenicity assay with TA98 strain, which is very sensitive 1-NP. The samples of MWCNT were able to bind to 1-NP therefore only free 1-NP molecules were able to enter the bacteria causing the mutagenic effect. The levels of the oxidation of the MWCNT modulated the mutagenicity of 1-NP. 1-NITROPYRENE (1-NP), WHICH IS MUTAGENIC AND CARCIONOGENIC, IS ONE OF THE MOST ABUNDANT NITRO POLYCYCLIC AROMATIC HYDROCARBON (NITRO-PAH) IN THE ENVIRONMENT. STRATEGIES TO REMEDIATE ORGANIC POLLUTANTS HAVE BEEN DEVELOPED AND NANOMATERIALS LIKE CARBON NANOTUBES (CNT) ARE ONE OF THEM. THEY PRESENT HIGH SPECIFIC SURFACE AREA, AN USEFUL PROPERTY FOR MOLECULE ADSORPTION. NITRIC ACID TREATMENT CAN INTRODUCE OXYGENATED GROUPS (E.G. CARBOXYLIC ACIDS) ON THE CNT SURFACES INCREASING WATER SOLUBILITY BUT DECREASING THE ABILITY OF CNT TO INTERACT WITH ORGANIC MOLECULES. WE USED SAMPLES OF ACID-TREATED MWCNT TO INVESTIGATE THE ABILITY OF CNT TO ADSORB 1-NP. DIFERENT DOSES OF WELL CHARACTERIZED CNTS WERE TESTED AGAINST DIFERENT DOSES OF 1-NP AND THE DETECTION OF THE NON-ADSORBED 1-NP WAS PERFORMED WITH THE SALMONELLA/MICROSOME MUTAGENICITY ASSAY WITH TA98 STRAIN, WHICH IS VERY SENSITIVE 1-NP. THE SAMPLES OF MWCNT WERE ABLE TO BIND TO 1-NP THEREFORE ONLY FREE 1-NP MOLECULES WERE ABLE TO ENTER THE BACTERIA CAUSING THE MUTAGENIC EFFECT. THE LEVELS OF THE OXIDATION OF THE MWCNT MODULATED THE MUTAGENICITY OF 1-NP. Posters: Layout: -Organizar seções para facilitar a leitura -Usar espaços em branco - Use listas de 2, 3 ou 4 itens (maiores os leitores esquecem....) - Use blocos com poucas linhas Posters: Estilo: -Inclua figuras, esquemas, representações gráficas, etc.... -Use listas verticais em vez de parágrafos longos - Aceite o fato que o poster não deve conter tantos detalhes como o artigo Para casa: Forneça cópias do poster (folha A4) http://www.swarthmore.edu/NatSci/cpurrin1/posteradvice.htm Exemplo de ilustração combinada com gráfico Atraem o Leitor AVP (median, 1st, 3rd quartile) 0 10 20 30 40 50 60 70 80 90 pre 30 60 90 120 post A V P ( p g /m l) control colic * jpg png Atenção para a resolução de figuras!!! I’ve fallen, and I can’t get up Exemplo de posters “bons” e “ruins” http://www.cns.cornell.edu/documents/ScientificPosters.pdf Uma lâmpada, por favor ! Oh my gawd! http://www.cns.cornell.edu/documents/ScientificPosters.pdf Um óculos escuro, por favor ! Where do I begin? http://www.cns.cornell.edu/documents/ScientificPosters.pdf Gorgeous! http://www.cns.cornell.edu/documents/ScientificPosters.pdf -Informação para contato -Foto Gorgeous! Perfect! http://www.cns.cornell.edu/documents/ScientificPosters.pdf Cooling Effects of Dirt Purge Holes on the Tips of Gas Turbine Blades The project goal was to find the film cooling effects of these dirt purge holes In summary, dirt purge holes provide cooling to the tip surface While intended to remove dirt from the blade, dirt purge holes also provide cooling to the tip surface. This cooling is enhanced with a small tip gap as the dirt purge floods the tip region near the leading edge with cool air. Acknowledgments The sponsor for this project was Pratt & Whitney. Eric Couch, Jesse Christophel, Erik Hohlfeld, and Karen Thole Gas turbine engines run better at higher combustion temperatures At higher combustion temperatures, these engines generate more power and use less fuel. However, these temperatures are restricted by melting temperatures of the turbine blades downstream of the combustor (see Figure 1). To find the effects, we performed wind tunnel experiments with scaled turbine blades. The wind tunnel was low speed and low temperature, and the blades, shown in Figure 3, were scaled at 12 times their normal size. To measure temperatures on the blade tip, we used an infrared camera. Tip gap sizes and amount of coolant flow from the dirt purge holes were both varied. Figure 3. Large-scale turbine blade in wind tunnel. Figure 4. Measurements of film cooling effectiveness. 0.19%0.10% 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 ! 0.29% 0.38% Large Tip Gap Small Tip Gap Blowing Ratio: Temperature measurements were converted to dimensionless cooling effectiveness c aw TT TT ! " " # $ $ Effectiveness where T$ = mainstream temperature Tc = coolant temperature Taw = adiabatic wall temperature (on tip surface) Figure 2. Flow at the tip region of a turbine blade. [IHPTET pamphlet, 2000] Dirt purge holes on turbine blade tips allow for higher combustion temperatures Harmful hot gases from the combustor leak across the gap between the blade tip and the shroud (see Figure 2). Dirt purge holes expel foreign particles from the blade tip so that film cooling holes are not blocked. Combustor T > 2500%C Figure 1. Pratt & Whitney F119 gas turbine engine. Turbine Section Tmelting point = 1000%C Cooling increased with blowing ratio The effectiveness contours of Figure 4 show that cooling increased with blowing ratio. 0.0 0.2 0.4 0.6 0.8 1.0 0.0 0.2 0.4 0.6 0.8 1.0 Small Tip, 0.10% Small Tip, 0.19% Small Tip, 0.29% Small Tip, 0.38% Large Tip, 0.10% Large Tip, 0.19% Large Tip, 0.29% Large Tip, 0.38%! X/Bx y x Small Tip, 0.38% Blowing Large Tip, 0.19% Blowing Figure 5. Laterally averaged effectiveness plotted against normalized axial chord. Tip size dramatically affected cooling In Figure 5, the lateral averages of effectiveness plotted against the axial chord length show that tip size dramatically affected the cooling. http://www.writing.engr.psu.edu/posters.html BO M A. Gargett and J. Wells Center for Coastal Physical Oceanography Old Dominion University 768 W 52nd St. Norfolk VA 23507 USA ABSTRACT ACKNOWLEDGEMENTS Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna ali- quam erat volutpat. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna ali- quam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna ali- quam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna ali- quam erat volutpat. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud. OBSERVATIONAL SETTING Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud.Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea com- modo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim qui blandit praesent luptatum zzril delenit augue duis dolore te feugait nulla facilisi. Lorem ipsum dolor sit amet, con- sectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud. ismod tincidunt ut laoreet dolore magna aliquam erat volutpat quis nostrud. Ut wisi enim ad minim veniam, quis nostrud.Lorem ipsum dolor sit amet, consectetuer adipiscing elit, sed diam nonummy nibh euismod tincidunt ut laoreet dolore magna aliquam erat volutpat. Ut wisi enim ad minim veniam, quis nostrud exerci tation ullamcorper suscipit lobortis nisl ut aliquip ex ea commodo consequat. Duis autem vel eum iriure dolor in hendrerit in vulputate velit esse molestie consequat, vel illum dolore eu feugiat nulla facilisis at vero eros et accumsan et iusto odio dignissim
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